hydroxo(5,10,15,20-tetrakis(mesityl)porphyrinato)iron(III)

Base Information

Chemical Name:hydroxo(5,10,15,20-tetrakis(mesityl)porphyrinato)iron(III)
CAS No.:77439-20-4
Molecular Formula:C₅₆H₅₃FeN₄O
Molecular Weight:853.91
Hs Code.:

Synonyms:hydroxo(5,10,15,20-tetrakis(mesityl)porphyrinato)iron(III)

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Chemical Property of hydroxo(5,10,15,20-tetrakis(mesityl)porphyrinato)iron(III)

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Technology Process of hydroxo(5,10,15,20-tetrakis(mesityl)porphyrinato)iron(III)

There total 6 articles about hydroxo(5,10,15,20-tetrakis(mesityl)porphyrinato)iron(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 136096-56-5,77439-21-5
5,10,15,20-tetra(2',4',6'-trimethylphenyl)porphyrinatoiron(III) chloride

: 7732-18-5
water

: 77439-20-4
hydroxo(5,10,15,20-tetrakis(mesityl)porphyrinato)iron(III)

Guidance literature:: With basic alumina; In dichloromethane; 10 wt % H2O on alumina; evapn. (vac.),;
DOI:10.1021/ja992373+

Reference yield: 78.0%

: 136096-56-5,77439-21-5
5,10,15,20-tetra(2',4',6'-trimethylphenyl)porphyrinatoiron(III) chloride

: 77439-20-4
hydroxo(5,10,15,20-tetrakis(mesityl)porphyrinato)iron(III)

Guidance literature:: With potassium hydroxide; In toluene; shaking of a soln. of porphinato-iron(III)-chloride in toluene with aq.KOH-soln. for 15h, the two phases were separated, the toluene phase waswashed with H2O, toluene was evaporated, residue was dissolved in acetone, dropwise addn. of H2O formed ppt.;; filtration, washed with water, dried at 50°C and 0.1 Torr;;

Reference yield:

: 75-91-2
tert.-butylhydroperoxide

: 81567-13-7
iron(II) meso-tetramesitylporphyrin

: 77439-20-4
hydroxo(5,10,15,20-tetrakis(mesityl)porphyrinato)iron(III)

: 122923-87-9
(tetramesitylporphine^(2-))FeOO-t-Bu

: 75-65-0
tert-butyl alcohol

Guidance literature:: In 2,2,4-trimethylpentane; ⁽²⁾H₈-toluene; Fe-compd. in d8-toluene placed in an NMR tube, cooled to -78°C, addn. of t-BuOOH in 2,2,4-trimethylpentane via a microsyringe at -78°C; followed by NMR spectroscopy;
DOI:10.1021/ja00202a021