2,2'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis-[1H-isoindole-1,3(2H)-dione]

Base Information

Chemical Name:2,2'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis-[1H-isoindole-1,3(2H)-dione]
CAS No.:949086-96-8
Molecular Formula:C₂₆H₁₉N₃O₅
Molecular Weight:453.454
Hs Code.:

Synonyms:2,2'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis-[1H-isoindole-1,3(2H)-dione]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis-[1H-isoindole-1,3(2H)-dione]

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Technology Process of 2,2'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis-[1H-isoindole-1,3(2H)-dione]

There total 1 articles about 2,2'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis-[1H-isoindole-1,3(2H)-dione] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1074-82-4
potassium phtalimide

: 188125-86-2
1,3-dichloropropan-2-one O-benzyloxime

: 949086-96-8
2,2'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis-[1H-isoindole-1,3(2H)-dione]

Guidance literature:: In N,N-dimethyl-formamide; at 100 ℃;
DOI:10.1016/j.tet.2007.05.109

Reference yield:

: 949086-96-8
2,2'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis-[1H-isoindole-1,3(2H)-dione]

: 949086-97-9
1,3-diamino-propan-2-one O-benzyloxime

Guidance literature:: With hydrazine hydrate; In methanol; for 3h; Heating;
DOI:10.1016/j.tet.2007.05.109

Reference yield:

: 949086-96-8
2,2'-{2-[(benzyloxy)imino]propane-1,3-diyl}bis-[1H-isoindole-1,3(2H)-dione]

: 949087-05-2
N,N'-{2-[(benzyloxy)imino]propane-1,3-diyl}-bis[(2R)-2,3-dihydroxypropanamide]

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / methanol / 3 h / Heating

2: 4.9 g / triethylamine; 4-dimethylaminopyridine / CH₂Cl₂

3: 100 percent / D,L-camphorsulfonic acid / ethanol / 3 h / Heating

With dmap; camphor-10-sulfonic acid; hydrazine hydrate; triethylamine; In methanol; ethanol; dichloromethane;
DOI:10.1016/j.tet.2007.05.109