1-octen-1-al <(1R,2S)-2-(dimethylamino)-1-phenylpropyl> trimethylsilyl acetal

Base Information

Chemical Name:1-octen-1-al <(1R,2S)-2-(dimethylamino)-1-phenylpropyl> trimethylsilyl acetal
CAS No.:114264-03-8
Molecular Formula:C₂₂H₃₉NO₂Si
Molecular Weight:377.643
Hs Code.:

Synonyms:1-octen-1-al <(1R,2S)-2-(dimethylamino)-1-phenylpropyl> trimethylsilyl acetal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-octen-1-al <(1R,2S)-2-(dimethylamino)-1-phenylpropyl> trimethylsilyl acetal

Chemical Property:

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Technology Process of 1-octen-1-al <(1R,2S)-2-(dimethylamino)-1-phenylpropyl> trimethylsilyl acetal

There total 3 articles about 1-octen-1-al <(1R,2S)-2-(dimethylamino)-1-phenylpropyl> trimethylsilyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 114264-02-7
(1R,2S)-2-(dimethylamino)-1-phenylpropyl octanoate

: 114264-03-8
1-octen-1-al <(1R,2S)-2-(dimethylamino)-1-phenylpropyl> trimethylsilyl acetal

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h;
DOI:10.1002/hlca.19870700522

Reference yield:

: 552-79-4
(-)-N-methylephedrine

: 114264-03-8
1-octen-1-al <(1R,2S)-2-(dimethylamino)-1-phenylpropyl> trimethylsilyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 89.2 percent / various solvent(s) / 72 h / Ambient temperature

2: BuLi / tetrahydrofuran / 1 h / -78 °C

With n-butyllithium; In tetrahydrofuran;
DOI:10.1002/hlca.19870700522

Reference yield:

: 111-64-8
n-octanoic acid chloride

: 114264-03-8
1-octen-1-al <(1R,2S)-2-(dimethylamino)-1-phenylpropyl> trimethylsilyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: 89.2 percent / various solvent(s) / 72 h / Ambient temperature

2: BuLi / tetrahydrofuran / 1 h / -78 °C

With n-butyllithium; In tetrahydrofuran;
DOI:10.1002/hlca.19870700522