4-(4-benzoylphenoxy)-N-(3-(5-(dimethylamino)naphthalene-1-sulfonamido)propyl)-N,N-dimethylbutan-1-ammonium bromide

Base Information

Chemical Name:4-(4-benzoylphenoxy)-N-(3-(5-(dimethylamino)naphthalene-1-sulfonamido)propyl)-N,N-dimethylbutan-1-ammonium bromide
CAS No.:1572037-54-7
Molecular Formula:Br*C₃₄H₄₂N₃O₄S
Molecular Weight:668.695
Hs Code.:

Synonyms:4-(4-benzoylphenoxy)-N-(3-(5-(dimethylamino)naphthalene-1-sulfonamido)propyl)-N,N-dimethylbutan-1-ammonium bromide

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Chemical Property of 4-(4-benzoylphenoxy)-N-(3-(5-(dimethylamino)naphthalene-1-sulfonamido)propyl)-N,N-dimethylbutan-1-ammonium bromide

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Technology Process of 4-(4-benzoylphenoxy)-N-(3-(5-(dimethylamino)naphthalene-1-sulfonamido)propyl)-N,N-dimethylbutan-1-ammonium bromide

There total 3 articles about 4-(4-benzoylphenoxy)-N-(3-(5-(dimethylamino)naphthalene-1-sulfonamido)propyl)-N,N-dimethylbutan-1-ammonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 30003-07-7
5-(dimethylamino)-N-(3-(dimethylamino)propyl)naphthalene-1-sulfonamide

4-[(4-bromobutyl)oxy]benzophenone: 101308-54-7
4-[(4-bromobutyl)oxy]benzophenone

: 1572037-54-7
4-(4-benzoylphenoxy)-N-(3-(5-(dimethylamino)naphthalene-1-sulfonamido)propyl)-N,N-dimethylbutan-1-ammonium bromide

Guidance literature:: In acetonitrile; at 100 ℃; for 24h; Temperature; Time;
DOI:10.1039/c3tb21633k

Reference yield:

: 1137-42-4
4-Hydroxybenzophenone

: 1572037-54-7
4-(4-benzoylphenoxy)-N-(3-(5-(dimethylamino)naphthalene-1-sulfonamido)propyl)-N,N-dimethylbutan-1-ammonium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 24 h / Reflux

2: acetonitrile / 24 h / 100 °C

With potassium carbonate; In acetonitrile; 2: |Menshutkin Reaction;
DOI:10.1039/c3tb21633k

Reference yield:

: 605-65-2
5-(dimethylamino)naphth-1-ylsulfonyl chloride

: 1572037-54-7
4-(4-benzoylphenoxy)-N-(3-(5-(dimethylamino)naphthalene-1-sulfonamido)propyl)-N,N-dimethylbutan-1-ammonium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 1 h / 23 °C / Inert atmosphere; Reflux

2: acetonitrile / 24 h / 100 °C

With triethylamine; In dichloromethane; acetonitrile; 2: |Menshutkin Reaction;
DOI:10.1039/c3tb21633k