ethyl 6-cyclohexylamino-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-L-glycero-α-D-galacto-octopyranuronate

Base Information

Chemical Name:ethyl 6-cyclohexylamino-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-L-glycero-α-D-galacto-octopyranuronate
CAS No.:696627-87-9
Molecular Formula:C₂₂H₃₇NO₇
Molecular Weight:427.538
Hs Code.:

Synonyms:ethyl 6-cyclohexylamino-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-L-glycero-α-D-galacto-octopyranuronate

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Chemical Property of ethyl 6-cyclohexylamino-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-L-glycero-α-D-galacto-octopyranuronate

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Technology Process of ethyl 6-cyclohexylamino-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-L-glycero-α-D-galacto-octopyranuronate

There total 3 articles about ethyl 6-cyclohexylamino-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-L-glycero-α-D-galacto-octopyranuronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4933-77-1
(3aR,5S,5aR,8aS,8bR)-2,2,7,7-Tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-carbaldehyde

: 696627-87-9
ethyl 6-cyclohexylamino-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-L-glycero-α-D-galacto-octopyranuronate

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / lithium hydroxide monohydrate / tetrahydrofuran / 10 h

2: ethanol / 22 h / 30 °C

With lithium hydroxide; In tetrahydrofuran; ethanol;
DOI:10.1081/CAR-120030140

Reference yield:

: 4064-06-6
1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

: 696627-87-9
ethyl 6-cyclohexylamino-6,7-dideoxy-1,2:3,4-di-O-isopropylidene-L-glycero-α-D-galacto-octopyranuronate

Guidance literature:: Multi-step reaction with 3 steps

1: 56.4 percent / pyridinium chlorochromate; molecular sieves 4 Angstroem / CH₂Cl₂ / 2 h

2: 85 percent / lithium hydroxide monohydrate / tetrahydrofuran / 10 h

3: ethanol / 22 h / 30 °C

With lithium hydroxide; 4 A molecular sieve; pyridinium chlorochromate; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1081/CAR-120030140