p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

Base Information

Chemical Name:p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside
CAS No.:359686-12-7
Molecular Formula:C₃₀H₃₄O₁₂
Molecular Weight:586.593
Hs Code.:

Synonyms:p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

Chemical Property:

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Technology Process of p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

There total 3 articles about p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 83-87-4,604-68-2,604-69-3,2152-77-4,4026-35-1,4163-59-1,4163-60-4,4163-61-5,4163-65-9,4257-94-7,4257-96-9,16299-15-3,19186-39-1,19189-55-0,25878-60-8,25941-03-1,32445-48-0,32445-49-1,32445-53-7,32445-54-8,34685-58-0,34685-59-1,43168-42-9,43168-44-1,43169-22-8,43169-25-1,66966-07-2,70749-17-6,80184-01-6,93221-01-3,93221-02-4,99630-88-3,109215-53-4,115792-70-6,115792-73-9,139894-92-1,139973-25-4,144071-49-8,147648-81-5
D-Mannose pentaacetate

: 31770-76-0
3-(4-hydroxyphenyl)propionic acid benzyl ester

: 359686-12-7
p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1081/CAR-100103953

Reference yield:

: 501-97-3
4-hydroxyphenylpropionic acid

: 359686-12-7
p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 765 mg / KHCO₃ / dimethylformamide / 12 h / 20 °C

2: 83 percent / Me₃SiOTf; molecular sieves 4 Angstroem / CH₂Cl₂ / 16 h / 20 °C

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; potassium hydrogencarbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1081/CAR-100103953

Reference yield:

: 100-39-0
benzyl bromide

: 359686-12-7
p-[2-(benzyloxycarbonyl)ethyl]phenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 765 mg / KHCO₃ / dimethylformamide / 12 h / 20 °C

2: 83 percent / Me₃SiOTf; molecular sieves 4 Angstroem / CH₂Cl₂ / 16 h / 20 °C

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; potassium hydrogencarbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1081/CAR-100103953