Nocardia heterobactin

Base Information

Chemical Name:Nocardia heterobactin
CAS No.:1202365-63-6
Molecular Formula:C₂₆H₃₁N₅O₁₀
Molecular Weight:573.56
Hs Code.:

Synonyms:Nocardia heterobactin

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Chemical Property of Nocardia heterobactin

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Technology Process of Nocardia heterobactin

There total 10 articles about Nocardia heterobactin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1304495-13-3
N,N'-[(R)-5-[[2-[[(S)-1-(benzyloxy)-2-oxopiperidin-3-yl]amino]-2-oxoethyl]amino]-5-oxopentane-1,4-diyl]bis[2,3-bis(benzyloxy)benzamide]

: 1202365-63-6
Nocardia heterobactin

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; for 6h; under 760.051 Torr;
DOI:10.1016/j.tet.2011.03.003

Reference yield:

: 74272-78-9
2,3-dibenzyloxybenzoic acid

: 1202365-63-6
Nocardia heterobactin

Guidance literature:: Multi-step reaction with 6 steps

1.1: dicyclohexyl-carbodiimide / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.1: potassium hydrogencarbonate / tetrahydrofuran; water / 24 h / 20 °C / pH 8 / Inert atmosphere

3.1: 1,1'-carbonyldiimidazole / dichloromethane / 1 h / 20 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: triethylsilane / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

5.1: triethylamine / water; acetonitrile / 40 h / 20 °C / Inert atmosphere

6.1: palladium 10% on activated carbon; hydrogen / methanol / 6 h / 760.05 Torr

With triethylsilane; palladium 10% on activated carbon; hydrogen; potassium hydrogencarbonate; triethylamine; dicyclohexyl-carbodiimide; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.tet.2011.03.003

Reference yield:

: 96920-81-9
2,3-bis(benzyloxy)benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester

: 1202365-63-6
Nocardia heterobactin

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydrogencarbonate / tetrahydrofuran; water / 24 h / 20 °C / pH 8 / Inert atmosphere

2.1: 1,1'-carbonyldiimidazole / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: triethylsilane / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

4.1: triethylamine / water; acetonitrile / 40 h / 20 °C / Inert atmosphere

5.1: palladium 10% on activated carbon; hydrogen / methanol / 6 h / 760.05 Torr

With triethylsilane; palladium 10% on activated carbon; hydrogen; potassium hydrogencarbonate; triethylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.tet.2011.03.003