(E)-N,N-diallyl-2-(2-(3,4-dimethylphenyl)hydrazono)-4-(thiophen-2-yl)butanamide

Base Information

Chemical Name:(E)-N,N-diallyl-2-(2-(3,4-dimethylphenyl)hydrazono)-4-(thiophen-2-yl)butanamide
CAS No.:1313027-25-6
Molecular Formula:C₂₂H₂₇N₃OS
Molecular Weight:381.542
Hs Code.:

Synonyms:(E)-N,N-diallyl-2-(2-(3,4-dimethylphenyl)hydrazono)-4-(thiophen-2-yl)butanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N,N-diallyl-2-(2-(3,4-dimethylphenyl)hydrazono)-4-(thiophen-2-yl)butanamide

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Technology Process of (E)-N,N-diallyl-2-(2-(3,4-dimethylphenyl)hydrazono)-4-(thiophen-2-yl)butanamide

There total 2 articles about (E)-N,N-diallyl-2-(2-(3,4-dimethylphenyl)hydrazono)-4-(thiophen-2-yl)butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 5834-04-8
3-(2-thienyl)-propanoic acid chloride

: 2192-34-9
3,4-(dimethyl)benzenediazonium tetrafluoroborate

: 124-02-7
diallylamine

: 1313027-25-6
(E)-N,N-diallyl-2-(2-(3,4-dimethylphenyl)hydrazono)-4-(thiophen-2-yl)butanamide

Guidance literature:: 3-(2-thienyl)-propanoic acid chloride; 3,4-(dimethyl)benzenediazonium tetrafluoroborate; With pyridine; In dichloromethane; at 20 ℃; for 2h;

diallylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/ejoc.201100261

Reference yield:

: 5928-51-8
3-(2-thienyl)propanoic acid

: 1313027-25-6
(E)-N,N-diallyl-2-(2-(3,4-dimethylphenyl)hydrazono)-4-(thiophen-2-yl)butanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

2.1: pyridine / dichloromethane / 2 h / 20 °C

2.2: 2 h / 20 °C

With pyridine; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1002/ejoc.201100261

Reference yield: 62.0%

: 1313027-25-6
(E)-N,N-diallyl-2-(2-(3,4-dimethylphenyl)hydrazono)-4-(thiophen-2-yl)butanamide

: 1313027-38-1
5-allyl-2-(3,4-dimethylphenyl)-6a-(2-(thiophen-2-yl)ethyl)-tetrahydropyrrolo[3,4-c]pyrazole-3,6(3aH,6aH)-dione

Guidance literature:: With copper diacetate; acetic acid; N,N-dimethyl-formamide; In water; at 80 ℃; for 9h; Inert atmosphere;
DOI:10.1002/ejoc.201100261