2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-hydroxy-3-phenylpropanal

Base Information

Chemical Name:2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-hydroxy-3-phenylpropanal
CAS No.:126741-89-7
Molecular Formula:C₂₆H₃₀O₂Si
Molecular Weight:402.609
Hs Code.:

Synonyms:2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-hydroxy-3-phenylpropanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-hydroxy-3-phenylpropanal

Chemical Property:

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Technology Process of 2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-hydroxy-3-phenylpropanal

There total 5 articles about 2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-hydroxy-3-phenylpropanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 201230-82-2
carbon monoxide

: 126741-76-2
(Z)-1-<(1',1'-dimethylethyl)diphenylsilyl>-3-phenylprop-1-en-3-ol

: 126741-89-7
2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-hydroxy-3-phenylpropanal

Guidance literature:: With carbonylhydridetris(triphenylphosphine)rhodium(I); hydrogen; triphenylphosphine; In benzene; at 80 ℃; for 66h; under 20685.9 Torr;

Reference yield:

: 100-52-7
benzaldehyde

: 126741-89-7
2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-hydroxy-3-phenylpropanal

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) butyllithium / 1.) hexane, THF, -78 deg C, 2 h, 2.) hexane, THF, RT, 7 h

2: 97 percent / H₂, quinoline / 10percent Pd/CaCO₃ / toluene / 760 Torr / Ambient temperature

3: 33 percent / H₂, carbonylhydridotris(triphenylphosphine)rhodium(I), triphenylphosphine / benzene / 66 h / 80 °C / 20685.9 Torr

With quinoline; carbonylhydridetris(triphenylphosphine)rhodium(I); n-butyllithium; hydrogen; triphenylphosphine; Lindlar's catalyst; In toluene; benzene;

Reference yield:

: 112440-16-1
1-<(1',1'-dimethylethyl)diphenylsilyl>acetylene

: 126741-89-7
2-<(1',1'-dimethylethyl)diphenylsilylmethyl>-3-hydroxy-3-phenylpropanal

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) butyllithium / 1.) hexane, THF, -78 deg C, 2 h, 2.) hexane, THF, RT, 7 h

2: 97 percent / H₂, quinoline / 10percent Pd/CaCO₃ / toluene / 760 Torr / Ambient temperature

3: 33 percent / H₂, carbonylhydridotris(triphenylphosphine)rhodium(I), triphenylphosphine / benzene / 66 h / 80 °C / 20685.9 Torr

With quinoline; carbonylhydridetris(triphenylphosphine)rhodium(I); n-butyllithium; hydrogen; triphenylphosphine; Lindlar's catalyst; In toluene; benzene;