4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide perchlorate

Base Information

• Chemical Name: 4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide perchlorate
• CAS No.: 1352569-82-4
• Molecular Formula: C₂₃H₂₀N₄O₂S*ClHO₄
• Molecular Weight: 516.962

Synonyms:4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide perchlorate

Chemical Property of 4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide perchlorate

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Technology Process of 4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide perchlorate

There total 2 articles about 4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

5-[methyl(phenyl)amino]-2-(4-nitrobenzyl)-3-p-tolyl-1,2,4-thiadiazolium perchlorate (1264264-01-8) → 4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide perchlorate (1352569-82-4)

Guidance literature:

at 190 ℃; for 0.666667h;

DOI:10.1134/S107036321110032X

Reference yield:

1-Methyl-3-{[(E)-4-nitro-benzylimino]-p-tolyl-methyl}-1-phenyl-thiourea (212254-00-7) → 4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide perchlorate (1352569-82-4)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; bromine / dichloromethane

2: 0.67 h / 190 °C

With pyridine; bromine; In dichloromethane;

DOI:10.1134/S107036321110032X

Reference yield: 88.0%

4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide perchlorate (1352569-82-4) → 4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide (670255-01-3)

Guidance literature:

With triethylamine; In tetrahydrofuran; for 4h;

DOI:10.1134/S107036321110032X

upstream raw materials:

5-[methyl(phenyl)amino]-2-(4-nitrobenzyl)-3-p-tolyl-1,2,4-thiadiazolium perchlorate

1-Methyl-3-{[(E)-4-nitro-benzylimino]-p-tolyl-methyl}-1-phenyl-thiourea

Downstream raw materials:

4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide

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