4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide

Base Information

Chemical Name:4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide
CAS No.:670255-01-3
Molecular Formula:C₂₃H₂₀N₄O₂S
Molecular Weight:416.503
Hs Code.:

Synonyms:4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide

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Chemical Property of 4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide

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Technology Process of 4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide

There total 3 articles about 4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1352569-82-4
4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide perchlorate

: 670255-01-3
4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide

Guidance literature:: With triethylamine; In tetrahydrofuran; for 4h;
DOI:10.1134/S107036321110032X

Reference yield:

: 1264264-01-8
5-[methyl(phenyl)amino]-2-(4-nitrobenzyl)-3-p-tolyl-1,2,4-thiadiazolium perchlorate

: 670255-01-3
4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide

Guidance literature:: Multi-step reaction with 2 steps

1: 0.67 h / 190 °C

2: triethylamine / tetrahydrofuran / 4 h

With triethylamine; In tetrahydrofuran;
DOI:10.1134/S107036321110032X

Reference yield:

: 212254-00-7
1-Methyl-3-{[(E)-4-nitro-benzylimino]-p-tolyl-methyl}-1-phenyl-thiourea

: 670255-01-3
4-methyl-N-[3-methyl-1,3-benzothiazol-2(3H)-ylidene]-N'-(4-nitrobenzyl)benzenecarboximidamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; bromine / dichloromethane

2: 0.67 h / 190 °C

3: triethylamine / tetrahydrofuran / 4 h

With pyridine; bromine; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1134/S107036321110032X