3,5-O-bis(tert-butyldimethylsilyl)-1-O-diphenylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol

Base Information

• Chemical Name: 3,5-O-bis(tert-butyldimethylsilyl)-1-O-diphenylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol
• CAS No.: 796883-95-9
• Molecular Formula: C₅₄H₇₃O₁₂PSi₂
• Molecular Weight: 1001.31

Synonyms:3,5-O-bis(tert-butyldimethylsilyl)-1-O-diphenylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol

Chemical Property of 3,5-O-bis(tert-butyldimethylsilyl)-1-O-diphenylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,5-O-bis(tert-butyldimethylsilyl)-1-O-diphenylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol

There total 3 articles about 3,5-O-bis(tert-butyldimethylsilyl)-1-O-diphenylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

tert-butyldimethylsilyl chloride (18162-48-6) + 1-O-diphenylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol (796883-94-8) → 3,5-O-bis(tert-butyldimethylsilyl)-1-O-diphenylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol (796883-95-9)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 50 ℃; for 46h;

DOI:10.1021/ja0466098

Reference yield:

chlorophosphoric acid diphenyl ester (2524-64-3) → 3,5-O-bis(tert-butyldimethylsilyl)-1-O-diphenylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol (796883-95-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / Et₃N; substituted His-Asn-His-Asn / toluene / 0 °C

2: 89 percent / imidazole / dimethylformamide

With 1H-imidazole; substituted His-Asn-His-Asn; triethylamine; In N,N-dimethyl-formamide; toluene;

DOI:10.1021/jo060702s

Reference yield:

2,4,6-tris-O-para-methoxybenzyl-myo-inositol (155666-58-3) → 3,5-O-bis(tert-butyldimethylsilyl)-1-O-diphenylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol (796883-95-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / Et₃N; substituted His-Asn-His-Asn / toluene / 0 °C

2: 89 percent / imidazole / dimethylformamide

With 1H-imidazole; substituted His-Asn-His-Asn; triethylamine; In N,N-dimethyl-formamide; toluene;

DOI:10.1021/jo060702s

upstream raw materials:

tert-butyldimethylsilyl chloride

1-O-diphenylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol

chlorophosphoric acid diphenyl ester

2,4,6-tris-O-para-methoxybenzyl-myo-inositol

Downstream raw materials:

3,5-O-bis(tert-butyldimethylsilyl)-1-O-dibenzylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol

1-O-dibenzylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 796883-95-9 3,5-O-bis(tert-butyldimethylsilyl)-1-O-diphenylphosphate-2,4,6-O-tri-para-methoxybenzyl-D-myo-inositol

Send

Send

Metric Ton KG G Pound L ML

Send

Send