thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside

Base Information

Chemical Name:thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside
CAS No.:402933-84-0
Molecular Formula:C₃₆H₄₄O₉Si
Molecular Weight:648.825
Hs Code.:

Synonyms:thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside

Chemical Property:

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Technology Process of thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside

There total 3 articles about thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 613-90-1
benzoyl cyanide

: 402933-90-8
thexyldimethylsilyl 4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside

: 402933-84-0
thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside

Guidance literature:: With triethylamine; In acetonitrile; for 2.5h;
DOI:10.1055/s-2001-18441

Reference yield:

: 701-99-5
Phenoxyacetyl chloride

: 402933-84-0
thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / pyridine / 2 h / -15 °C

2: 93 percent / Et₃N / acetonitrile / 2.5 h

With pyridine; triethylamine; In acetonitrile;
DOI:10.1055/s-2001-18441

Reference yield:

: 175980-93-5
(2S,4aR,6S,7R,8R,8aR)-6-[Dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol

: 402933-84-0
thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / pyridine / 2 h / -15 °C

2: 93 percent / Et₃N / acetonitrile / 2.5 h

With pyridine; triethylamine; In acetonitrile;
DOI:10.1055/s-2001-18441