thexyldimethylsilyl 4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside

Base Information

Chemical Name:thexyldimethylsilyl 4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside
CAS No.:402933-90-8
Molecular Formula:C₂₉H₄₀O₈Si
Molecular Weight:544.717
Hs Code.:

Synonyms:thexyldimethylsilyl 4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside

Suppliers and Price of thexyldimethylsilyl 4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of thexyldimethylsilyl 4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of thexyldimethylsilyl 4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside

There total 1 articles about thexyldimethylsilyl 4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 701-99-5
Phenoxyacetyl chloride

: 175980-93-5
(2S,4aR,6S,7R,8R,8aR)-6-[Dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol

: 402933-90-8
thexyldimethylsilyl 4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside

Guidance literature:: With pyridine; at -15 ℃; for 2h;
DOI:10.1055/s-2001-18441

Reference yield: 93.0%

: 613-90-1
benzoyl cyanide

: 402933-90-8
thexyldimethylsilyl 4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside

: 402933-84-0
thexyldimethylsilyl 2-O-benzoyl-4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside

Guidance literature:: With triethylamine; In acetonitrile; for 2.5h;
DOI:10.1055/s-2001-18441

Reference yield:

: 402933-90-8
thexyldimethylsilyl 4,6-O-benzylidene-3-O-phenoxyacetyl-β-D-galactopyranoside

: 402933-85-1
thexyldimethylsilyl 2-O-benzoyl-4-O-benzyl-3-O-phenoxyacetyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / Et₃N / acetonitrile / 2.5 h

2: 90 percent / BH₃*THF; dibutyl boron triflate / CH₂Cl₂ / 6 h

With borane-THF; di-n-butylboryl trifluoromethanesulfonate; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1055/s-2001-18441