C₂₉H₃₂N₂O₄

Base Information

Chemical Name:C₂₉H₃₂N₂O₄
CAS No.:1578270-88-8
Molecular Formula:C₂₉H₃₂N₂O₄
Molecular Weight:472.584
Hs Code.:

C<sub>29</sub>H<sub>32</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₉H₃₂N₂O₄

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Chemical Property of C₂₉H₃₂N₂O₄

Chemical Property:

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Technology Process of C₂₉H₃₂N₂O₄

There total 3 articles about C₂₉H₃₂N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 1557159-75-7
benzyl (6-((tert-butoxycarbonyl)amino)hexyl)(5-hydroxy-2-nitrobenzyl)carbamate

: 1578270-88-8
C₂₉H₃₂N₂O₄

Guidance literature:: benzyl (6-((tert-butoxycarbonyl)amino)hexyl)(5-hydroxy-2-nitrobenzyl)carbamate; With Merifield chloromethylstyrene resin; tetra-(n-butyl)ammonium iodide; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide; at 60 ℃; for 12h; under 150.015 Torr;

With cesium acetate; In dichloromethane; N,N-dimethyl-formamide; at 60 ℃; for 12h; under 150.015 Torr;

(fluorenylmethoxy)carbonyl chloride; Further stages;
DOI:10.1021/ol500530q

Reference yield:

: 1557159-77-9
C₁₈H₂₇N₃O₅

: 1578270-88-8
C₂₉H₃₂N₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate / methanol / 0.5 h / 25 °C

2.1: triethylamine / methanol / 1 h / 25 °C

2.2: 25 °C

3.1: Merifield chloromethylstyrene resin; caesium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide; dichloromethane / 12 h / 60 °C / 150.01 Torr

3.2: 12 h / 60 °C / 150.01 Torr

With sodium tetrahydroborate; Merifield chloromethylstyrene resin; tetra-(n-butyl)ammonium iodide; caesium carbonate; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol500530q

Reference yield:

: 1557159-80-4
C₁₈H₂₉N₃O₅

: 1578270-88-8
C₂₉H₃₂N₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / methanol / 1 h / 25 °C

1.2: 25 °C

2.1: Merifield chloromethylstyrene resin; caesium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide; dichloromethane / 12 h / 60 °C / 150.01 Torr

2.2: 12 h / 60 °C / 150.01 Torr

With Merifield chloromethylstyrene resin; tetra-(n-butyl)ammonium iodide; caesium carbonate; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol500530q