(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ethylzinc

Base Information

• Chemical Name: (2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ethylzinc
• CAS No.: 215808-47-2
• Molecular Formula: C₃₁H₄₆N₂Zn
• Molecular Weight: 512.11

Synonyms:(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ethylzinc

Chemical Property of (2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ethylzinc

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Technology Process of (2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ethylzinc

There total 2 articles about (2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ethylzinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

diethylzinc (557-20-0) + 2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-2-pentene → (2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ethylzinc (215808-47-2)

Guidance literature:

In hexane; toluene; at 80 ℃; Inert atmosphere;

DOI:10.1002/anie.202014960

Reference yield: 100.0%

diethylzinc (557-20-0) + 2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-2-pentene (289618-59-3) → (2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ethylzinc (215808-47-2)

Guidance literature:

In toluene; (N2); addn. of a soln. of ligand in toluene to a soln. of ZnEt2 in toluene at 0°C, stirring overnight at 80°C; drying in vac., crystn. at room temp. in glovebox;

DOI:10.1021/ja003850n

Reference yield: 100.0%

methanol (67-56-1) + (2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ethylzinc (215808-47-2) → [(((CH3)2CH)2C6H3NC(CH3)CHC(CH3)NC6H3(CH(CH3)2)2)Zn(OCH3)]2 (340026-17-7)

Guidance literature:

In toluene; (N2); addn. of methanol to a soln. of zinc complex in toluene at room temp., stirring for 1 h at room temp.; drying in vac.;

DOI:10.1021/ja003850n

upstream raw materials:

diethylzinc

2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-2-pentene

Downstream raw materials:

[(2-((2,6-diisopropylphenyl)amido)-4-((2,6-diisopropylphenyl)imino)-2-pentene)ZnOAc]2

[(((CH₃)2CH)2C₆H₃NC(CH₃)CHC(CH₃)NC₆H₃(CH(CH₃)2)2)Zn(OCH₃)]2

2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-2-pentene

[(((CH₃)2CH)2C₆H₃NC(CH₃)CHC(CH₃)NC₆H₃(CH(CH₃)2)2)Zn(O₂SC₂H₅)]2

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