2-[4,5-bis(pentylthio)-1,3-dithiol-2-ylidene]-4-benzoyl-1,3-dithiolo[4,5-c]pyrrole

Base Information

• Chemical Name: 2-[4,5-bis(pentylthio)-1,3-dithiol-2-ylidene]-4-benzoyl-1,3-dithiolo[4,5-c]pyrrole
• CAS No.: 1129427-85-5
• Molecular Formula: C₂₅H₂₉NOS₆
• Molecular Weight: 551.907

Synonyms:2-[4,5-bis(pentylthio)-1,3-dithiol-2-ylidene]-4-benzoyl-1,3-dithiolo[4,5-c]pyrrole

Chemical Property of 2-[4,5-bis(pentylthio)-1,3-dithiol-2-ylidene]-4-benzoyl-1,3-dithiolo[4,5-c]pyrrole

Chemical Property:

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Technology Process of 2-[4,5-bis(pentylthio)-1,3-dithiol-2-ylidene]-4-benzoyl-1,3-dithiolo[4,5-c]pyrrole

There total 1 articles about 2-[4,5-bis(pentylthio)-1,3-dithiol-2-ylidene]-4-benzoyl-1,3-dithiolo[4,5-c]pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

C30H49NS6 + benzoyl chloride (98-88-4) → 2-[4,5-bis(pentylthio)-1,3-dithiol-2-ylidene]-4-benzoyl-1,3-dithiolo[4,5-c]pyrrole (1129427-85-5)

Guidance literature:

C₃₀H₄₉NS₆; With ethylmagnesium bromide; In tetrahydrofuran; diethyl ether; at 20 ℃; for 0.583333h; Inert atmosphere;

benzoyl chloride; In tetrahydrofuran; diethyl ether; at 20 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1055/s-0031-1289739

Reference yield: 85.0%

2-[4,5-bis(pentylthio)-1,3-dithiol-2-ylidene]-4-benzoyl-1,3-dithiolo[4,5-c]pyrrole (1129427-85-5) + methyl iodide (74-88-4) → 5-methyl-2-[4,5-bis(pentylthio)-1,3-dithiole-2-yliden]-(1,3)-dithiolo[4,5-c]pyrrole-4-yl-phenylmethanone

Guidance literature:

2-[4,5-bis(pentylthio)-1,3-dithiol-2-ylidene]-4-benzoyl-1,3-dithiolo[4,5-c]pyrrole; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.5h; Inert atmosphere;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; for 1h; Inert atmosphere;

DOI:10.1055/s-0031-1289739

Reference yield: 77.0%

2-[4,5-bis(pentylthio)-1,3-dithiol-2-ylidene]-4-benzoyl-1,3-dithiolo[4,5-c]pyrrole (1129427-85-5) + 1-iodo-propane (107-08-4) → 5-propyl-2-[4,5-bis(pentylthio)-1,3-dithiole-2-yliden]-(1,3)-dithiolo[4,5-c]pyrrole-4-yl-phenylmethanone

Guidance literature:

2-[4,5-bis(pentylthio)-1,3-dithiol-2-ylidene]-4-benzoyl-1,3-dithiolo[4,5-c]pyrrole; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.5h; Inert atmosphere;

1-iodo-propane; In N,N-dimethyl-formamide; mineral oil; for 24h; Inert atmosphere;

DOI:10.1055/s-0031-1289739

upstream raw materials:

benzoyl chloride

Downstream raw materials:

C₂₅H₃₁NOS₆

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