(S)-2-(dibenzylamino)-N'-methoxy-4,N'-dimethylpentane amide

Base Information

Chemical Name:(S)-2-(dibenzylamino)-N'-methoxy-4,N'-dimethylpentane amide
CAS No.:131150-36-2
Molecular Formula:C₂₂H₃₀N₂O₂
Molecular Weight:354.492
Hs Code.:

Synonyms:(S)-2-(dibenzylamino)-N'-methoxy-4,N'-dimethylpentane amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-(dibenzylamino)-N'-methoxy-4,N'-dimethylpentane amide

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Technology Process of (S)-2-(dibenzylamino)-N'-methoxy-4,N'-dimethylpentane amide

There total 5 articles about (S)-2-(dibenzylamino)-N'-methoxy-4,N'-dimethylpentane amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 95084-25-6
(S)-2-dibenzylamino-4-methylpentanoic acid

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 131150-36-2
(S)-2-(dibenzylamino)-N'-methoxy-4,N'-dimethylpentane amide

Guidance literature:: With 1,1'-carbonyldiimidazole; In tetrahydrofuran; at 0 - 25 ℃; for 4h; Solvent; Concentration;

Reference yield: 84.0%

: 189562-54-7
methyl N,N-dibenzyl-L-leucinate

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 131150-36-2
(S)-2-(dibenzylamino)-N'-methoxy-4,N'-dimethylpentane amide

Guidance literature:: N,O-dimethylhydroxylamine*hydrochloride; With isopropylmagnesium chloride; In tetrahydrofuran; at 0 ℃; for 0.25h;

methyl N,N-dibenzyl-L-leucinate; In tetrahydrofuran; at 0 - 20 ℃; for 7h;
DOI:10.1016/j.tet.2015.02.014

Reference yield:

: 61-90-5,21675-61-6,25248-98-0,70-45-1
L-leucine

: 131150-36-2
(S)-2-(dibenzylamino)-N'-methoxy-4,N'-dimethylpentane amide

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / methanol / 3 h / 0 °C / Reflux

1.2: 1 h / 0 °C

1.3: 12 h / 0 - 20 °C

2.1: isopropylmagnesium chloride / tetrahydrofuran / 0.25 h / 0 °C

2.2: 7 h / 0 - 20 °C

With thionyl chloride; isopropylmagnesium chloride; In tetrahydrofuran; methanol;
DOI:10.1016/j.tet.2015.02.014