(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) chloride

Base Information

Chemical Name:(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) chloride
CAS No.:1445971-88-9
Molecular Formula:C₃₄H₃₁ClP₂Pd
Molecular Weight:643.441
Hs Code.:

Synonyms:(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) chloride

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Chemical Property of (2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) chloride

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Technology Process of (2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) chloride

There total 3 articles about (2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 21264-30-2,90243-59-7,14592-56-4
dichloro bis(acetonitrile) palladium(II)

: 1445947-50-1
1,5-bis((diphenylphosphinoyl)methyl)-2,4-dimethylbenzene

: 1445971-88-9
(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) chloride

Guidance literature:: 1,5-bis((diphenylphosphinoyl)methyl)-2,4-dimethylbenzene; With trichlorosilane; triethylamine; In toluene; for 18h; Reflux;

dichloro bis(acetonitrile) palladium(II); In toluene; for 10h; Reflux;
DOI:10.1021/ol401560q

Reference yield:

: 4559-70-0
Diphenylphosphine oxide

: 1445971-88-9
(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C

2.1: triethylamine; trichlorosilane / toluene / 18 h / Reflux

2.2: 10 h / Reflux

With trichlorosilane; sodium hydride; triethylamine; In tetrahydrofuran; toluene; mineral oil;
DOI:10.1021/ol401560q

Reference yield:

: 1585-15-5
4,6-bis(chloromethyl)-m-xylene

: 1445971-88-9
(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) chloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C

2.1: triethylamine; trichlorosilane / toluene / 18 h / Reflux

2.2: 10 h / Reflux

With trichlorosilane; sodium hydride; triethylamine; In tetrahydrofuran; toluene; mineral oil;
DOI:10.1021/ol401560q