acetoxy(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II)

Base Information

Chemical Name:acetoxy(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II)
CAS No.:1445971-87-8
Molecular Formula:C₃₆H₃₄O₂P₂Pd
Molecular Weight:667.032
Hs Code.:

Synonyms:acetoxy(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II)

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Chemical Property of acetoxy(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II)

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Technology Process of acetoxy(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II)

There total 4 articles about acetoxy(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1445971-88-9
(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) chloride

: 563-63-3
silver(I) acetate

: 1445971-87-8
acetoxy(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II)

Guidance literature:: In dichloromethane; at 20 ℃; for 24h; Inert atmosphere; Darkness;
DOI:10.1021/ol401560q

Reference yield:

: 4559-70-0
Diphenylphosphine oxide

: 1445971-87-8
acetoxy(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II)

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C

2.1: triethylamine; trichlorosilane / toluene / 18 h / Reflux

2.2: 10 h / Reflux

3.1: dichloromethane / 24 h / 20 °C / Inert atmosphere; Darkness

With trichlorosilane; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; toluene; mineral oil;
DOI:10.1021/ol401560q

Reference yield:

: 1585-15-5
4,6-bis(chloromethyl)-m-xylene

: 1445971-87-8
acetoxy(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II)

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C

2.1: triethylamine; trichlorosilane / toluene / 18 h / Reflux

2.2: 10 h / Reflux

3.1: dichloromethane / 24 h / 20 °C / Inert atmosphere; Darkness

With trichlorosilane; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; toluene; mineral oil;
DOI:10.1021/ol401560q