1-(aquapalladium(II))-2,6-bis((diphenylphosphino)methyl)-3,5-dimethylbenzene trifluoromethylsulfonate

Base Information

Chemical Name:1-(aquapalladium(II))-2,6-bis((diphenylphosphino)methyl)-3,5-dimethylbenzene trifluoromethylsulfonate
CAS No.:1445971-92-5
Molecular Formula:CF₃O₃S*C₃₄H₃₃OP₂Pd
Molecular Weight:775.073
Hs Code.:

Synonyms:1-(aquapalladium(II))-2,6-bis((diphenylphosphino)methyl)-3,5-dimethylbenzene trifluoromethylsulfonate

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Chemical Property of 1-(aquapalladium(II))-2,6-bis((diphenylphosphino)methyl)-3,5-dimethylbenzene trifluoromethylsulfonate

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Technology Process of 1-(aquapalladium(II))-2,6-bis((diphenylphosphino)methyl)-3,5-dimethylbenzene trifluoromethylsulfonate

There total 4 articles about 1-(aquapalladium(II))-2,6-bis((diphenylphosphino)methyl)-3,5-dimethylbenzene trifluoromethylsulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1445971-88-9
(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) chloride

: 7732-18-5
water

: 2923-28-6
silver trifluoromethanesulfonate

: 1445971-92-5
1-(aquapalladium(II))-2,6-bis((diphenylphosphino)methyl)-3,5-dimethylbenzene trifluoromethylsulfonate

Guidance literature:: In acetone; at 20 ℃; for 2h; Darkness;
DOI:10.1021/ol401560q

Reference yield:

: 4559-70-0
Diphenylphosphine oxide

: 1445971-92-5
1-(aquapalladium(II))-2,6-bis((diphenylphosphino)methyl)-3,5-dimethylbenzene trifluoromethylsulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C

2.1: triethylamine; trichlorosilane / toluene / 18 h / Reflux

2.2: 10 h / Reflux

3.1: acetone / 2 h / 20 °C / Darkness

With trichlorosilane; sodium hydride; triethylamine; In tetrahydrofuran; acetone; toluene; mineral oil;
DOI:10.1021/ol401560q

Reference yield:

: 1585-15-5
4,6-bis(chloromethyl)-m-xylene

: 1445971-92-5
1-(aquapalladium(II))-2,6-bis((diphenylphosphino)methyl)-3,5-dimethylbenzene trifluoromethylsulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C

2.1: triethylamine; trichlorosilane / toluene / 18 h / Reflux

2.2: 10 h / Reflux

3.1: acetone / 2 h / 20 °C / Darkness

With trichlorosilane; sodium hydride; triethylamine; In tetrahydrofuran; acetone; toluene; mineral oil;
DOI:10.1021/ol401560q