(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) iodide

Base Information

Chemical Name:(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) iodide
CAS No.:1445971-89-0
Molecular Formula:C₃₄H₃₁IP₂Pd
Molecular Weight:734.892
Hs Code.:

Synonyms:(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) iodide

Suppliers and Price of (2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) iodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) iodide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) iodide

There total 4 articles about (2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1445971-88-9
(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) chloride

: 7681-11-0
potassium iodide

: 1445971-89-0
(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) iodide

Guidance literature:: In methanol; dichloromethane; at 20 ℃;
DOI:10.1021/ol401560q

Reference yield:

: 4559-70-0
Diphenylphosphine oxide

: 1445971-89-0
(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) iodide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C

2.1: triethylamine; trichlorosilane / toluene / 18 h / Reflux

2.2: 10 h / Reflux

3.1: methanol; dichloromethane / 20 °C

With trichlorosilane; sodium hydride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; toluene; mineral oil;
DOI:10.1021/ol401560q

Reference yield:

: 1585-15-5
4,6-bis(chloromethyl)-m-xylene

: 1445971-89-0
(2,6-bis((diphenylphosphino)methyl)-3,5-dimethylphenyl)palladium(II) iodide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

1.2: 18 h / 20 °C

2.1: triethylamine; trichlorosilane / toluene / 18 h / Reflux

2.2: 10 h / Reflux

3.1: methanol; dichloromethane / 20 °C

With trichlorosilane; sodium hydride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; toluene; mineral oil;
DOI:10.1021/ol401560q