C₁₄H₁₀BrClO₃

Base Information

Chemical Name:C₁₄H₁₀BrClO₃
CAS No.:1254343-49-1
Molecular Formula:C₁₄H₁₀BrClO₃
Molecular Weight:341.589
Hs Code.:

C<sub>14</sub>H<sub>10</sub>BrClO<sub>3</sub>

Synonyms:C₁₄H₁₀BrClO₃

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Chemical Property of C₁₄H₁₀BrClO₃

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Technology Process of C₁₄H₁₀BrClO₃

There total 10 articles about C₁₄H₁₀BrClO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1254340-86-7
phenyl 4-bromo-3-chloro-6-methoxy-2-methylbenzoate

: 1254343-49-1
C₁₄H₁₀BrClO₃

Guidance literature:: phenyl 4-bromo-3-chloro-6-methoxy-2-methylbenzoate; With boron tribromide; In dichloromethane; at -78 - 0 ℃; for 0.75h;

With sodium hydrogencarbonate; In dichloromethane; water; at 20 ℃; for 0.166667h;

Reference yield:

: 877149-08-1
4-bromo-2-methoxy-6-methyl-benzoic acid

: 1254343-49-1
C₁₄H₁₀BrClO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

2.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

3.1: N-chloro-succinimide / acetonitrile / 45 h / 60 °C

4.1: boron tribromide / dichloromethane / 0.75 h / -78 - 0 °C

4.2: 0.17 h / 20 °C

With dmap; N-chloro-succinimide; oxalyl dichloride; boron tribromide; triethylamine; N,N-dimethyl-formamide; In dichloromethane; acetonitrile;

Reference yield:

: 877149-05-8
4-bromo-2-methoxy-6-methyl-benzonitrile

: 1254343-49-1
C₁₄H₁₀BrClO₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: diisobutylaluminium hydride / toluene; tetrahydrofuran / -78 - 20 °C

1.2: 0 - 20 °C

2.1: 2-methyl-but-2-ene; water; sodium chlorite; sodium dihydrogenphosphate / tert-butyl alcohol / 0.5 h / 20 °C

2.2: pH 1

3.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 0.5 h / 20 °C

4.1: dmap; triethylamine / dichloromethane / 1 h / 20 °C

5.1: N-chloro-succinimide / acetonitrile / 45 h / 60 °C

6.1: boron tribromide / dichloromethane / 0.75 h / -78 - 0 °C

6.2: 0.17 h / 20 °C

With dmap; sodium chlorite; sodium dihydrogenphosphate; N-chloro-succinimide; 2-methyl-but-2-ene; oxalyl dichloride; water; boron tribromide; diisobutylaluminium hydride; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; toluene; acetonitrile; tert-butyl alcohol;