benzyl 4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4yl)propyl)(hexyl)amino)ethoxy)phenyl)butylcarbamate

Base Information

Chemical Name:benzyl 4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4yl)propyl)(hexyl)amino)ethoxy)phenyl)butylcarbamate
CAS No.:1416973-54-0
Molecular Formula:C₃₉H₅₄N₂O₈
Molecular Weight:678.866
Hs Code.:

Synonyms:benzyl 4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4yl)propyl)(hexyl)amino)ethoxy)phenyl)butylcarbamate

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Chemical Property of benzyl 4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4yl)propyl)(hexyl)amino)ethoxy)phenyl)butylcarbamate

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Technology Process of benzyl 4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4yl)propyl)(hexyl)amino)ethoxy)phenyl)butylcarbamate

There total 3 articles about benzyl 4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4yl)propyl)(hexyl)amino)ethoxy)phenyl)butylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 25152-90-3
(4aR,6S,7R,8R,8aS)-2-phenylhexahydropyrano[3,2-d][1,3]dioxine-6,7,8-triol

: 587880-59-9
{4-[4-(2-Aminoethoxy)phenyl]butyl}carbamic acid benzyl ester hydrochloride

: 66-25-1
hexanal

: 1416973-54-0
benzyl 4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4yl)propyl)(hexyl)amino)ethoxy)phenyl)butylcarbamate

Guidance literature:: (4aR,6S,7R,8R,8aS)-2-phenylhexahydropyrano[3,2-d][1,3]dioxine-6,7,8-triol; {4-[4-(2-Aminoethoxy)phenyl]butyl}carbamic acid benzyl ester hydrochloride; With acetic acid; In methanol; at 20 ℃; for 2h;

With sodium cyanoborohydride; In methanol; at 20 ℃;

hexanal; In methanol; at 20 ℃;

Reference yield:

: 587880-55-5
{4-[4-(2-tert-Butoxycarbonylaminoethoxy)phenyl]butyl}carbamic acid benzyl ester

: 1416973-54-0
benzyl 4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4yl)propyl)(hexyl)amino)ethoxy)phenyl)butylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

2.1: acetic acid / methanol / 2 h / 20 °C

2.2: 20 °C

2.3: 20 °C

With hydrogenchloride; acetic acid; In 1,4-dioxane; methanol;

Reference yield:

: 587880-25-9
4-(4-hydroxyphenyl)butylcarbamic acid benzyl ester

: 1416973-54-0
benzyl 4-(4-(2-(((2S,3R)-2,3-dihydroxy-3-((4R,5R)-5-hydroxy-2-phenyl-1,3-dioxan-4yl)propyl)(hexyl)amino)ethoxy)phenyl)butylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

2.1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

3.1: acetic acid / methanol / 2 h / 20 °C

3.2: 20 °C

3.3: 20 °C

With hydrogenchloride; di-isopropyl azodicarboxylate; acetic acid; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; methanol;