di-tert-butyl 6-(4-((1-(2-fluoroethyl )-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methyl-5,6-dihydrophenanthridine-3,8-diyldicarbamate

Base Information

Chemical Name:di-tert-butyl 6-(4-((1-(2-fluoroethyl )-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methyl-5,6-dihydrophenanthridine-3,8-diyldicarbamate
CAS No.:1314081-08-7
Molecular Formula:C₃₅H₄₁FN₆O₅
Molecular Weight:644.746
Hs Code.:

Synonyms:di-tert-butyl 6-(4-((1-(2-fluoroethyl )-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methyl-5,6-dihydrophenanthridine-3,8-diyldicarbamate

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Chemical Property of di-tert-butyl 6-(4-((1-(2-fluoroethyl )-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methyl-5,6-dihydrophenanthridine-3,8-diyldicarbamate

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Technology Process of di-tert-butyl 6-(4-((1-(2-fluoroethyl )-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methyl-5,6-dihydrophenanthridine-3,8-diyldicarbamate

There total 11 articles about di-tert-butyl 6-(4-((1-(2-fluoroethyl )-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methyl-5,6-dihydrophenanthridine-3,8-diyldicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 894792-94-0
1-azido-2-fluoroethane

: 1314081-07-6
di-tert-butyl (5-methyl-6-(4-(prop-2-yn-1-yloxy)phenyl)-5,6-dihydrophenanthridine-3,8-diyl)dicarbamate

: 1314081-08-7
di-tert-butyl 6-(4-((1-(2-fluoroethyl )-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methyl-5,6-dihydrophenanthridine-3,8-diyldicarbamate

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In N,N-dimethyl-formamide; at 23 ℃; Inert atmosphere;
DOI:10.1039/c3ob42379d

Reference yield:

: 100-07-2
4-methoxy-benzoyl chloride

: 1314081-08-7
di-tert-butyl 6-(4-((1-(2-fluoroethyl )-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methyl-5,6-dihydrophenanthridine-3,8-diyldicarbamate

Guidance literature:: Multi-step reaction with 10 steps

1: chlorobenzene / Reflux

2: ammonium formate / 20 % Pd(OH)2/C

4: trichlorophosphate

5: hydrogen bromide / water

7: potassium carbonate / acetone

8: tetrahydrofuran

9: sodium cyanoborohydride

10: sodium L-ascorbate; copper(II) sulfate / N,N-dimethyl-formamide

With hydrogen bromide; ammonium formate; sodium cyanoborohydride; potassium carbonate; copper(II) sulfate; sodium L-ascorbate; trichlorophosphate; 20 % Pd(OH)2/C; In tetrahydrofuran; water; N,N-dimethyl-formamide; chlorobenzene; acetone;

Reference yield:

: 51787-75-8
4,4'-dinitro-2-biphenylamine

: 1314081-08-7
di-tert-butyl 6-(4-((1-(2-fluoroethyl )-1H-1,2,3-triazol-4-yl)methoxy)phenyl)-5-methyl-5,6-dihydrophenanthridine-3,8-diyldicarbamate

Guidance literature:: Multi-step reaction with 10 steps

1: chlorobenzene / Reflux

2: ammonium formate / 20 % Pd(OH)2/C

4: trichlorophosphate

5: hydrogen bromide / water

7: potassium carbonate / acetone

8: tetrahydrofuran

9: sodium cyanoborohydride

10: sodium L-ascorbate; copper(II) sulfate / N,N-dimethyl-formamide

With hydrogen bromide; ammonium formate; sodium cyanoborohydride; potassium carbonate; copper(II) sulfate; sodium L-ascorbate; trichlorophosphate; 20 % Pd(OH)2/C; In tetrahydrofuran; water; N,N-dimethyl-formamide; chlorobenzene; acetone;