di-tert-butyl (5-methyl-6-(4-(prop-2-yn-1-yloxy)phenyl)-5,6-dihydrophenanthridine-3,8-diyl)dicarbamate

Base Information

Chemical Name:di-tert-butyl (5-methyl-6-(4-(prop-2-yn-1-yloxy)phenyl)-5,6-dihydrophenanthridine-3,8-diyl)dicarbamate
CAS No.:1314081-07-6
Molecular Formula:C₃₃H₃₇N₃O₅
Molecular Weight:555.674
Hs Code.:

Synonyms:di-tert-butyl (5-methyl-6-(4-(prop-2-yn-1-yloxy)phenyl)-5,6-dihydrophenanthridine-3,8-diyl)dicarbamate

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Chemical Property of di-tert-butyl (5-methyl-6-(4-(prop-2-yn-1-yloxy)phenyl)-5,6-dihydrophenanthridine-3,8-diyl)dicarbamate

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Technology Process of di-tert-butyl (5-methyl-6-(4-(prop-2-yn-1-yloxy)phenyl)-5,6-dihydrophenanthridine-3,8-diyl)dicarbamate

There total 10 articles about di-tert-butyl (5-methyl-6-(4-(prop-2-yn-1-yloxy)phenyl)-5,6-dihydrophenanthridine-3,8-diyl)dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1314081-06-5
3,8-bis(tert-butoxycarbonylamino)-5-methyl-6-(4-( prop-2-ynyloxy)phenyl)phenanthridinium iodide

: 1314081-07-6
di-tert-butyl (5-methyl-6-(4-(prop-2-yn-1-yloxy)phenyl)-5,6-dihydrophenanthridine-3,8-diyl)dicarbamate

Guidance literature:: With sodium cyanoborohydride; In methanol; at 23 ℃; for 3h; Inert atmosphere;
DOI:10.1039/c3ob42379d

Reference yield:

: 100-07-2
4-methoxy-benzoyl chloride

: 1314081-07-6
di-tert-butyl (5-methyl-6-(4-(prop-2-yn-1-yloxy)phenyl)-5,6-dihydrophenanthridine-3,8-diyl)dicarbamate

Guidance literature:: Multi-step reaction with 9 steps

1: chlorobenzene / Reflux

2: ammonium formate / 20 % Pd(OH)2/C

4: trichlorophosphate

5: hydrogen bromide / water

7: potassium carbonate / acetone

8: tetrahydrofuran

9: sodium cyanoborohydride

With hydrogen bromide; ammonium formate; sodium cyanoborohydride; potassium carbonate; trichlorophosphate; 20 % Pd(OH)2/C; In tetrahydrofuran; water; chlorobenzene; acetone;

Reference yield:

: 51787-75-8
4,4'-dinitro-2-biphenylamine

: 1314081-07-6
di-tert-butyl (5-methyl-6-(4-(prop-2-yn-1-yloxy)phenyl)-5,6-dihydrophenanthridine-3,8-diyl)dicarbamate

Guidance literature:: Multi-step reaction with 9 steps

1: chlorobenzene / Reflux

2: ammonium formate / 20 % Pd(OH)2/C

4: trichlorophosphate

5: hydrogen bromide / water

7: potassium carbonate / acetone

8: tetrahydrofuran

9: sodium cyanoborohydride

With hydrogen bromide; ammonium formate; sodium cyanoborohydride; potassium carbonate; trichlorophosphate; 20 % Pd(OH)2/C; In tetrahydrofuran; water; chlorobenzene; acetone;