3-butyrylbenzonitrile

Base Information

Chemical Name:3-butyrylbenzonitrile
CAS No.:50916-35-3
Molecular Formula:C₁₁H₁₁NO
Molecular Weight:173.214
Hs Code.:

Synonyms:3-butyrylbenzonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-butyrylbenzonitrile

Chemical Property:

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Technology Process of 3-butyrylbenzonitrile

There total 5 articles about 3-butyrylbenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 6952-59-6
3-cyanobromobenzene

: 123-72-8
butyraldehyde

: 50916-35-3
3-butyrylbenzonitrile

Guidance literature:: With nickel(II) iodide; potassium phosphate; tetrakis(tetrabutylammonium)decatungstate(VI); 4,4'-di-tert-butyl-2,2'-bipyridine; In acetonitrile; at 20 ℃; for 4h; Schlenk technique; Inert atmosphere; Irradiation;
DOI:10.1021/acs.orglett.0c01121

Reference yield: 60.0%

: 626-17-5
benzene-1,3-dicarbonitrile

: 107-08-4
1-iodo-propane

: 50916-35-3
3-butyrylbenzonitrile

Guidance literature:: With nickel(II) iodide; samarium diiodide; In tetrahydrofuran; at 0 - 20 ℃; for 2h;
DOI:10.1016/S0040-4039(99)02194-2

Reference yield:

: 2234-82-4
1-propylmagnesium chloride

: 1711-11-1
3-cyanobenzoyl chloride

: 50916-35-3
3-butyrylbenzonitrile

Guidance literature:: 1-propylmagnesium chloride; With bis[(2-(N,N-dimethylaminoethyl))]ether; In tetrahydrofuran; diethyl ether; at 0 ℃; for 0.25h;

3-cyanobenzoyl chloride; In tetrahydrofuran; diethyl ether; at -60 ℃;
DOI:10.1002/anie.201609963