2,3,4,5,6-pentafluoroformanilide

Base Information

• Chemical Name: 2,3,4,5,6-pentafluoroformanilide
• CAS No.: 58751-08-9
• Molecular Formula: C₇H₂F₅NO
• Molecular Weight: 211.091
• Mol file: 58751-08-9.mol

Synonyms:2,3,4,5,6-pentafluoroformanilide

Chemical Property of 2,3,4,5,6-pentafluoroformanilide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3,4,5,6-pentafluoroformanilide

There total 7 articles about 2,3,4,5,6-pentafluoroformanilide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

formic acid (64-18-6) + N-(2,3,4,5,6-pentafluorophenyl)-1-phenylmethanimine (143896-70-2,63400-36-2) → 2,3,4,5,6-pentafluoroformanilide (58751-08-9) + benzoic acid (65-85-0,8013-63-6)

Guidance literature:

With dihydrogen peroxide;

DOI:10.1016/S0022-1139(00)85191-X

Reference yield: 56.0%

formic acid (64-18-6) + 2,3,4,5,6-pentafluoroaniline (771-60-8) → 2,3,4,5,6-pentafluoroformanilide (58751-08-9)

Guidance literature:

In para-xylene; at 100 ℃; for 67h;

DOI:10.1002/jlcr.1670

Reference yield: 55.0%

2,3,4,5,6-pentafluoroaniline (771-60-8) + sodium hydride (7646-69-7) + formic acid ethyl ester (109-94-4) → 2,3,4,5,6-pentafluoroformanilide (58751-08-9)

Guidance literature:

In tetrahydrofuran; Mixing at -10 - (-20)°C then added HCOOC2H5 at 20°C.; Sublimation or crystallization from CCl4 leads to modification A, crystallization from melt to modification B.;

upstream raw materials:

formic acid

2,3,4,5,6-pentafluoroaniline

N-(2,3,4,5,6-pentafluorophenyl)-1-phenylmethanimine

N,N-dimethyl-formamide

Downstream raw materials:

N-(pentafluorophenyl)carbonimidoyl dichloride

N,N′-bis(pentafluorophenyl)methanimidamine

2,3,4,5,6-pentafluorophenyl isocyanide

N-formyl-N,N'-decafluorodiphenyl-tetrafluoro-1,4-phenylene-diamine