sodium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Base Information

Chemical Name:sodium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate
CAS No.:1200445-81-3
Molecular Formula:C₂₄H₂₁ClNO₄*Na
Molecular Weight:445.878
Hs Code.:

Synonyms:sodium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

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Chemical Property of sodium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Chemical Property:

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Technology Process of sodium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

There total 11 articles about sodium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 578-22-3
2-methyl-5-hydroxybenzoic acid

: 1200445-81-3
sodium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 - 80 °C

2: water; lithium hydroxide / 1,4-dioxane / 20 °C / Inert atmosphere

3: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

4: triethylamine / dichloromethane / 20 °C

5: hydrogenchloride; water; acetic acid / 2 h / 90 °C

6: sodium hydroxide / methanol / 20 °C / Sonographic reaction

With hydrogenchloride; oxalyl dichloride; water; potassium carbonate; acetic acid; triethylamine; N,N-dimethyl-formamide; sodium hydroxide; lithium hydroxide; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1034025-63-2
(4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetic acid

: 1200445-81-3
sodium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Guidance literature:: With sodium hydroxide; In methanol; at 20 ℃; Sonographic reaction;

Reference yield:

: 446-33-3
5-Fluoro-2-nitrotoluene

: 1200445-81-3
sodium (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 20 °C / Cooling with ice

1.2: 88 h / 20 - 100 °C / Inert atmosphere

2.1: hydrogen / palladium 10% on activated carbon / ethanol / 760.05 Torr

3.1: triethylamine / dichloromethane / 20 °C

4.1: hydrogenchloride; water; acetic acid / 2 h / 90 °C

5.1: sodium hydroxide / methanol / 20 °C / Sonographic reaction

With hydrogenchloride; water; hydrogen; sodium hydride; acetic acid; triethylamine; sodium hydroxide; palladium 10% on activated carbon; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;