(4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetic acid

Base Information

Chemical Name:(4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetic acid
CAS No.:1034025-63-2
Molecular Formula:C₂₄H₂₂ClNO₄
Molecular Weight:423.896
Hs Code.:

Synonyms:(4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetic acid

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Chemical Property of (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetic acid

Chemical Property:

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Technology Process of (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetic acid

There total 11 articles about (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 578-22-3
2-methyl-5-hydroxybenzoic acid

: 1034025-63-2
(4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 - 80 °C

2: water; lithium hydroxide / 1,4-dioxane / 20 °C / Inert atmosphere

3: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

4: triethylamine / dichloromethane / 20 °C

5: hydrogenchloride; water; acetic acid / 2 h / 90 °C

With hydrogenchloride; oxalyl dichloride; water; potassium carbonate; acetic acid; triethylamine; N,N-dimethyl-formamide; lithium hydroxide; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1034026-35-1
ethyl (4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetate

: 1034025-63-2
(4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetic acid

Guidance literature:: With hydrogenchloride; water; acetic acid; at 20 - 90 ℃; Product distribution / selectivity;

Reference yield:

: 1028543-03-4
ethyl phenylmethyl [3-methyl-4-nitrophenyl]propanedioate

: 1034025-63-2
(4-{[(5-{[(3-chlorophenyl)methyl]oxy}-2-methylphenyl)carbonyl]amino}-3-methylphenyl)acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / ethanol / 760.05 Torr

2: triethylamine / dichloromethane / 20 °C

3: hydrogenchloride; water; acetic acid / 2 h / 90 °C

With hydrogenchloride; water; hydrogen; acetic acid; triethylamine; palladium 10% on activated carbon; In ethanol; dichloromethane;