N-(bis(perfluorophenyl)phosphoryl)-P,P-bis(perfluorophenyl)phosphinic amide

Base Information

Chemical Name:N-(bis(perfluorophenyl)phosphoryl)-P,P-bis(perfluorophenyl)phosphinic amide
CAS No.:844658-81-7
Molecular Formula:C₂₄HF₂₀NO₂P₂
Molecular Weight:777.193
Hs Code.:

Synonyms:N-(bis(perfluorophenyl)phosphoryl)-P,P-bis(perfluorophenyl)phosphinic amide

Suppliers and Price of N-(bis(perfluorophenyl)phosphoryl)-P,P-bis(perfluorophenyl)phosphinic amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of N-(bis(perfluorophenyl)phosphoryl)-P,P-bis(perfluorophenyl)phosphinic amide

Chemical Property:

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

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Hazard Codes:

MSDS Files:

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Technology Process of N-(bis(perfluorophenyl)phosphoryl)-P,P-bis(perfluorophenyl)phosphinic amide

There total 3 articles about N-(bis(perfluorophenyl)phosphoryl)-P,P-bis(perfluorophenyl)phosphinic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 5032-90-6
chlorobis(pentafluorophenyl)phosphane

: 844658-81-7
N-(bis(perfluorophenyl)phosphoryl)-P,P-bis(perfluorophenyl)phosphinic amide

Guidance literature:: chlorobis(pentafluorophenyl)phosphane; With 1,1,1,3,3,3-hexamethyl-disilazane; In benzene; for 16h; Reflux;

With dibenzoyl peroxide; In tetrahydrofuran; at 5 - 15 ℃; for 10h; Reagent/catalyst; Solvent; Temperature;

Reference yield:

: 344-04-7
bromopentafluorobenzene

: 844658-81-7
N-(bis(perfluorophenyl)phosphoryl)-P,P-bis(perfluorophenyl)phosphinic amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: Mg; iodine / diethyl ether / 2 h / Heating

1.2: 54 percent / phosphorus tribromide / diethyl ether / 1 h

2.1: toluene / 5 h / Heating

3.1: 0.98 g / aq. hydrogen peroxide / toluene; tetrahydrofuran

With dihydrogen peroxide; iodine; magnesium; In tetrahydrofuran; diethyl ether; toluene;
DOI:10.1002/chem.200700087

Reference yield:

: 13648-79-8
bis(pentafluorophenyl)bromophosphine

: 844658-81-7
N-(bis(perfluorophenyl)phosphoryl)-P,P-bis(perfluorophenyl)phosphinic amide

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 5 h / Heating

2: 0.98 g / aq. hydrogen peroxide / toluene; tetrahydrofuran

With dihydrogen peroxide; In tetrahydrofuran; toluene;
DOI:10.1002/chem.200700087