α-(ethoxycarbonyl)-4-methoxybenzyl alcohol pentafluorobenzoate ester

Base Information

Chemical Name:α-(ethoxycarbonyl)-4-methoxybenzyl alcohol pentafluorobenzoate ester
CAS No.:136878-05-2
Molecular Formula:C₁₈H₁₃F₅O₅
Molecular Weight:404.29
Hs Code.:

Synonyms:α-(ethoxycarbonyl)-4-methoxybenzyl alcohol pentafluorobenzoate ester

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Chemical Property of α-(ethoxycarbonyl)-4-methoxybenzyl alcohol pentafluorobenzoate ester

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Technology Process of α-(ethoxycarbonyl)-4-methoxybenzyl alcohol pentafluorobenzoate ester

There total 2 articles about α-(ethoxycarbonyl)-4-methoxybenzyl alcohol pentafluorobenzoate ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 602-94-8
Pentafluorobenzoic acid

: 36141-66-9
ethyl 2-hydroxy-2-(4-methoxyphenyl)acetate

: 136878-05-2
α-(ethoxycarbonyl)-4-methoxybenzyl alcohol pentafluorobenzoate ester

Guidance literature:: With 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In diethyl ether; for 3h; Ambient temperature;
DOI:10.1021/jo00074a036

Reference yield:

: 20714-90-3
4-Methoxymandelic acid

: 136878-05-2
α-(ethoxycarbonyl)-4-methoxybenzyl alcohol pentafluorobenzoate ester

Guidance literature:: Multi-step reaction with 2 steps

1: 32 percent / p-toluenesulfonic acid / 4 h / Heating

2: 59 percent / DCC, 4-pyrrolidinopyridine / diethyl ether / 3 h / Ambient temperature

With 4-pyrrolidin-1-ylpyridine; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In diethyl ether;
DOI:10.1021/jo00074a036