(-)-menthyl (E)-1,2-diphenylpropenoate

Base Information

Chemical Name:(-)-menthyl (E)-1,2-diphenylpropenoate
CAS No.:144788-96-5
Molecular Formula:C₂₅H₃₀O₂
Molecular Weight:362.512
Hs Code.:

Synonyms:(-)-menthyl (E)-1,2-diphenylpropenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-menthyl (E)-1,2-diphenylpropenoate

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Technology Process of (-)-menthyl (E)-1,2-diphenylpropenoate

There total 2 articles about (-)-menthyl (E)-1,2-diphenylpropenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.7%

: 2216-51-5
(-)-menthol

: 58085-33-9
α-phenyl-cinnamoyl chloride

: 144788-96-5
(-)-menthyl (E)-1,2-diphenylpropenoate

Guidance literature:: With magnesium; In toluene;
DOI:10.1016/0022-328X(92)83365-O

Reference yield:

: 91-48-5
(E)-2,3-diphenylpropenoic acid

: 19139-34-5,144788-96-5
2,3t-diphenyl-acrylic acid-((1R)-menthyl ester)

Guidance literature:: With phosphorus trichloride; benzene; man setzt das Chlorid mit l-Menthol in Benzol in Gegenwart von Pyridin um;

Reference yield:

: (-)-menthyldimethyltin hydride

: 144788-96-5
(-)-menthyl (E)-1,2-diphenylpropenoate

: (-)-menthyl 2,3-diphenyl-3-((-)-menthyldimethylstannyl)propanoate

Guidance literature:: With catalyst: azobisisobutyronitrile; In not given; N2-atmosphere; excess of Sn-compd., 85°C, 48 h; diastereomer mixt. partly sepd. by chromy. (SiO2, 3% AcOEt in light petroleum; giving 91.7% erythro-diastereomers in resulting mixt.); (1)H-, (13)C-, (119)Sn-NMR spectroscopy;
DOI:10.1016/S0022-328X(99)00278-8