4,5-dihydro-2-<2'-methoxy-4',6-bis(1-methylethoxy)<1,1'-biphenyl>-2-yl>-4,4-dimethyloxazole

Base Information

Chemical Name:4,5-dihydro-2-<2'-methoxy-4',6-bis(1-methylethoxy)<1,1'-biphenyl>-2-yl>-4,4-dimethyloxazole
CAS No.:176391-62-1
Molecular Formula:C₂₄H₃₁NO₄
Molecular Weight:397.514
Hs Code.:

Synonyms:4,5-dihydro-2-<2'-methoxy-4',6-bis(1-methylethoxy)<1,1'-biphenyl>-2-yl>-4,4-dimethyloxazole

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Chemical Property of 4,5-dihydro-2-<2'-methoxy-4',6-bis(1-methylethoxy)<1,1'-biphenyl>-2-yl>-4,4-dimethyloxazole

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Technology Process of 4,5-dihydro-2-<2'-methoxy-4',6-bis(1-methylethoxy)<1,1'-biphenyl>-2-yl>-4,4-dimethyloxazole

There total 4 articles about 4,5-dihydro-2-<2'-methoxy-4',6-bis(1-methylethoxy)<1,1'-biphenyl>-2-yl>-4,4-dimethyloxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 504-77-8
4,5-dihydro-1,3-oxazol

: 176391-62-1
4,5-dihydro-2-<2'-methoxy-4',6-bis(1-methylethoxy)<1,1'-biphenyl>-2-yl>-4,4-dimethyloxazole

Guidance literature:

Reference yield:

: 102127-34-4
4-bromo-3-methoxyphenol

: 176391-62-1
4,5-dihydro-2-<2'-methoxy-4',6-bis(1-methylethoxy)<1,1'-biphenyl>-2-yl>-4,4-dimethyloxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / K₂CO₃ / butan-2-one / 17 h / Heating

2: 1.) Mg, I₂, ethylene dibromide / 1.) THF, 50 deg C, 40 min, 2.) THF, 50 deg C

With iodine; potassium carbonate; magnesium; ethylene dibromide; In butanone;
DOI:10.1021/jo9601369

Reference yield:

: 114605-67-3
4,5-dihydro-2-<2,3-bis(1-methylethoxy)-1-phenyl>-4,4-dimethyloxazole

: 176391-61-0
1-bromo-4-isopropoxy-2-methoxybenzene

: 176391-62-1
4,5-dihydro-2-<2'-methoxy-4',6-bis(1-methylethoxy)<1,1'-biphenyl>-2-yl>-4,4-dimethyloxazole

Guidance literature:: With iodine; magnesium; ethylene dibromide; Yield given. Multistep reaction; 1.) THF, 50 deg C, 40 min, 2.) THF, 50 deg C;
DOI:10.1021/jo9601369