1'-phenyl-<1'-oxy>-2'-<<(1,1-dimethylethyl)dimethylsilyl>-oxy>ethane

Base Information

Chemical Name:1'-phenyl-<1'-oxy>-2'-<<(1,1-dimethylethyl)dimethylsilyl>-oxy>ethane
CAS No.:166248-63-1
Molecular Formula:C₁₉H₃₂O₃Si
Molecular Weight:336.547
Hs Code.:

1'-phenyl-<1'-<tetrahydropyranyl>oxy>-2'-<<(1,1-dimethylethyl)dimethylsilyl>-oxy>ethane

Synonyms:1'-phenyl-<1'-oxy>-2'-<<(1,1-dimethylethyl)dimethylsilyl>-oxy>ethane

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Chemical Property of 1'-phenyl-<1'-oxy>-2'-<<(1,1-dimethylethyl)dimethylsilyl>-oxy>ethane

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Technology Process of 1'-phenyl-<1'-oxy>-2'-<<(1,1-dimethylethyl)dimethylsilyl>-oxy>ethane

There total 8 articles about 1'-phenyl-<1'-oxy>-2'-<<(1,1-dimethylethyl)dimethylsilyl>-oxy>ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 110-87-2
3,4-dihydro-2H-pyran

: 71009-09-1
2-(tert-butyldimethylsilyl)oxy-1-phenylethanol

: 166248-63-1
1'-phenyl-<1'-oxy>-2'-<<(1,1-dimethylethyl)dimethylsilyl>-oxy>ethane

Guidance literature:: toluene-4-sulfonic acid; In dichloromethane; at 20 ℃; for 12h;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 166248-63-1
1'-phenyl-<1'-oxy>-2'-<<(1,1-dimethylethyl)dimethylsilyl>-oxy>ethane

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / imidazole / dimethylformamide / Ambient temperature

2: 92 percent / p-TsOH*H₂O / CH₂Cl₂ / Ambient temperature

With 1H-imidazole; toluene-4-sulfonic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)89330-3

Reference yield:

: 103548-04-5
2-(tert-butyldimethylsilanyloxy)-1-phenylethan-1-one

: 166248-63-1
1'-phenyl-<1'-oxy>-2'-<<(1,1-dimethylethyl)dimethylsilyl>-oxy>ethane

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate; methanol / 5.5 h / 20 °C

2: toluene-4-sulfonic acid / dichloromethane / 12 h / 20 °C

With methanol; sodium tetrahydroborate; toluene-4-sulfonic acid; In dichloromethane;