1,1,3,3-tetradiisopropylphenyl-1,1,3,3-tetrahydro-2,2-bi-1,3,2-diazaphosphole

Base Information

• Chemical Name: 1,1,3,3-tetradiisopropylphenyl-1,1,3,3-tetrahydro-2,2-bi-1,3,2-diazaphosphole
• CAS No.: 1151469-21-4
• Molecular Formula: C₅₂H₇₂N₄P₂
• Molecular Weight: 815.118

Synonyms:1,1,3,3-tetradiisopropylphenyl-1,1,3,3-tetrahydro-2,2-bi-1,3,2-diazaphosphole

Chemical Property of 1,1,3,3-tetradiisopropylphenyl-1,1,3,3-tetrahydro-2,2-bi-1,3,2-diazaphosphole

Chemical Property:

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Technology Process of 1,1,3,3-tetradiisopropylphenyl-1,1,3,3-tetrahydro-2,2-bi-1,3,2-diazaphosphole

There total 2 articles about 1,1,3,3-tetradiisopropylphenyl-1,1,3,3-tetrahydro-2,2-bi-1,3,2-diazaphosphole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2-chloro-1,3-bis(diisopropylphenyl)-1,3-dihydro-1,3,2-diazaphosphol (884639-92-3) → 1,1,3,3-tetradiisopropylphenyl-1,1,3,3-tetrahydro-2,2-bi-1,3,2-diazaphosphole (1151469-21-4)

Guidance literature:

With iodine; magnesium; In tetrahydrofuran; for 12h; Inert atmosphere; Schlenk technique;

DOI:10.1002/ejic.201200633

Reference yield:

2-hydrido-1,3-bis(2,6-diisopropylphenyl)-1,3,2-diazaphosphalene → 1,1,3,3-tetradiisopropylphenyl-1,1,3,3-tetrahydro-2,2-bi-1,3,2-diazaphosphole (1151469-21-4) + hydrogen (1333-74-0)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 24h; Photolysis; Inert atmosphere;

DOI:10.1002/anie.201504504

Reference yield: 65.0%

1,1,3,3-tetradiisopropylphenyl-1,1,3,3-tetrahydro-2,2-bi-1,3,2-diazaphosphole (1151469-21-4) + diphenyl acetylene (501-65-5) → C66H82N4P2 (1416042-58-4)

Guidance literature:

In tetrahydrofuran; at 50 ℃; for 12h; Schlenk technique; Inert atmosphere;

DOI:10.1002/ejic.201200633

upstream raw materials:

2-chloro-1,3-bis(diisopropylphenyl)-1,3-dihydro-1,3,2-diazaphosphol

Downstream raw materials:

C₂₆H₃₆N₂P

C₆₆H₈₂N₄P₂

2-chloro-1,3-bis(diisopropylphenyl)-1,3-dihydro-1,3,2-diazaphosphol

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