tert-butyl 2,3,4,6-tetra-O-benzyl-α-D-mannopyranoside

Base Information

Chemical Name:tert-butyl 2,3,4,6-tetra-O-benzyl-α-D-mannopyranoside
CAS No.:128745-66-4
Molecular Formula:C₃₈H₄₄O₆
Molecular Weight:596.764
Hs Code.:

Synonyms:tert-butyl 2,3,4,6-tetra-O-benzyl-α-D-mannopyranoside

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Chemical Property of tert-butyl 2,3,4,6-tetra-O-benzyl-α-D-mannopyranoside

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Technology Process of tert-butyl 2,3,4,6-tetra-O-benzyl-α-D-mannopyranoside

There total 90 articles about tert-butyl 2,3,4,6-tetra-O-benzyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.5%

: 371766-59-5
2,3,4,6-tetra-O-benzyl-1-O-[N-allyl-thiocarbamoyl]-D-glucopyranose

: 75-65-0
tert-butyl alcohol

: 78153-80-7,128745-66-4,128745-67-5,136984-90-2,136984-93-5,67525-69-3
tert-butyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

Guidance literature:: With bromine; sodium hydrogencarbonate; lithium fluoride; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; at -25 ℃; for 0.166667h;

Reference yield: 87.5%

: 75-65-0
tert-butyl alcohol

: 530114-05-7
2,3,4,6-tetra-O-benzyl-1-O-(N-allylthiocarbamoyl)-β-D-glucopyranose

: 78153-80-7,128745-66-4,128745-67-5,136984-90-2,136984-93-5,67525-69-3
tert-butyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

Guidance literature:: With bromine; sodium hydrogencarbonate; lithium trifluoromethanesulfonate; 4 A molecular sieve; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; at -25 ℃; for 0.166667h;

Reference yield: 86.0%

: 74808-09-6
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl trichloroacetimidate

: 75-65-0
tert-butyl alcohol

: 67525-69-3,128745-66-4,128745-67-5,136984-90-2,136984-93-5,78153-80-7
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-2-((benzyloxy)methyl)-6-(tert-butoxy)tetrahydro-2H-pyran

Guidance literature:: 2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl trichloroacetimidate; tert-butyl alcohol; In dichloromethane; at 20 ℃; for 0.0833333h; Inert atmosphere;

With tris(pentafluorophenyl)borate; In dichloromethane; at -10 ℃; for 1.5h; stereoselective reaction;
DOI:10.1021/acs.joc.8b00215