18H-tetrabenzo[a,c,h,j]phenoxazine

Base Information

• Chemical Name: 18H-tetrabenzo[a,c,h,j]phenoxazine
• CAS No.: 215-15-6
• Molecular Formula: C₂₈H₁₇NO
• Molecular Weight: 383.449
• Mol file: 215-15-6.mol

Synonyms:18H-tetrabenzo[a,c,h,j]phenoxazine

Chemical Property of 18H-tetrabenzo[a,c,h,j]phenoxazine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 18H-tetrabenzo[a,c,h,j]phenoxazine

There total 4 articles about 18H-tetrabenzo[a,c,h,j]phenoxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9,10-phenanthrenequinone (84-11-7) + benzylamine (100-46-9) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 2-phenylphenanthro[9,10-d]oxazole (4410-14-4) + benzaldehyde (100-52-7) + 18H-tetrabenzo[a,c,h,j]phenoxazine (215-15-6)

Guidance literature:

at 100 ℃;

DOI:10.1021/jo01189a008

Reference yield:

10-imino-10H-phenanthren-9-one (3942-85-6) + Hexamethylphosphorous triamide (1608-26-0) → N,N,N,N,N,N-hexamethylphosphoric triamide (680-31-9) + 9,10-phenanthrenequinone (84-11-7) + 18H-tetrabenzo[a,c,h,j]phenoxazine (215-15-6)

Guidance literature:

In benzene; at 5 ℃; for 0.166667h; Mechanism; Product distribution; other aminophosphines, other phenanthrene derivatives;

Reference yield:

phenanthrene-9,10-dione oxime (14140-04-6) → 10-amino-phenanthren-9-ol (55586-24-8) + 18H-tetrabenzo[a,c,h,j]phenoxazine (215-15-6)

Guidance literature:

With ethanol; hydrogen sulfide;

upstream raw materials:

phenanthrene-9,10-dione oxime

10-imino-10H-phenanthren-9-one

Hexamethylphosphorous triamide

acetic acid