N-ethyl-N-[1-oxo-4-[1-[(phenylmethoxy)carbonyl]-4-piperidinyl]butyl]glycine

Base Information

• Chemical Name: N-ethyl-N-[1-oxo-4-[1-[(phenylmethoxy)carbonyl]-4-piperidinyl]butyl]glycine
• CAS No.: 222640-99-5
• Molecular Formula: C₂₁H₃₀N₂O₅
• Molecular Weight: 390.48

Synonyms:N-ethyl-N-[1-oxo-4-[1-[(phenylmethoxy)carbonyl]-4-piperidinyl]butyl]glycine

Chemical Property of N-ethyl-N-[1-oxo-4-[1-[(phenylmethoxy)carbonyl]-4-piperidinyl]butyl]glycine

Chemical Property:

Purity/Quality:

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Technology Process of N-ethyl-N-[1-oxo-4-[1-[(phenylmethoxy)carbonyl]-4-piperidinyl]butyl]glycine

There total 2 articles about N-ethyl-N-[1-oxo-4-[1-[(phenylmethoxy)carbonyl]-4-piperidinyl]butyl]glycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

oxalyl dichloride (79-37-8) + 4-(1-((benzyloxy)carbonyl)piperidin-4-yl)butanoic acid (204139-61-7) + benzyl 4-(4-chloro-4-oxobutyl)piperidine-1-carboxylate + N-ethylglycine (627-01-0) → N-ethyl-N-[1-oxo-4-[1-[(phenylmethoxy)carbonyl]-4-piperidinyl]butyl]glycine (222640-99-5)

Guidance literature:

With sodium carbonate; In tetrahydrofuran; N-methyl-acetamide; dichloromethane; water; ethyl acetate; acetonitrile;

Reference yield:

N-ethyl-N-[1-oxo-4-[1-[(phenylmethoxy)carbonyl]-4-piperidinyl]butyl]glycine ethyl ester → N-ethyl-N-[1-oxo-4-[1-[(phenylmethoxy)carbonyl]-4-piperidinyl]butyl]glycine (222640-99-5)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran;

Reference yield: 95.0%

diisopropylethyl amine (861359-74-2) + (L)-α-aspartyl-3-cyclohexyl-(L-alanineamide phenylmethyl ester trifluoroacetate + N-ethyl-N-[1-oxo-4-[1-[(phenylmethoxy)carbonyl]-4-piperidinyl]butyl]glycine (222640-99-5) + O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate (125700-67-6) → N-[N-ethyl-N-[1-oxo-4-[1-[(phenylmethoxy)carbonyl]-4-piperidinyl]butyl]glycyl]-(L)-α-aspartyl-3-cyclohexyl-(L)-alanineamide phenylmethyl ester

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N-methyl-acetamide; N,N-dimethyl-formamide;

upstream raw materials:

oxalyl dichloride

4-(1-((benzyloxy)carbonyl)piperidin-4-yl)butanoic acid

N-ethylglycine

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