(5β,6α)-6-Hydroxy-3-oxo-cholan-24-oic Acid Methyl Ester

Base Information

Chemical Name:(5β,6α)-6-Hydroxy-3-oxo-cholan-24-oic Acid Methyl Ester
CAS No.:3360-89-2
Molecular Formula:C₂₅H₄₀O₄
Molecular Weight:404.59
Hs Code.:
Mol file:3360-89-2.mol

Synonyms:3α-oxo-6α-hydroxy-5β-cholan-24-oic acid methyl ester

Suppliers and Price of (5β,6α)-6-Hydroxy-3-oxo-cholan-24-oic Acid Methyl Ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
(5β,6α)-6-Hydroxy-3-oxo-cholan-24-oicAcidMethylEster
25mg
$ 165.00

Medical Isotopes, Inc.
(5β,6α)-6-Hydroxy-3-oxo-cholan-24-oicAcidMethylEster
250 mg
$ 2200.00

Total 3 raw suppliers

Chemical Property of (5β,6α)-6-Hydroxy-3-oxo-cholan-24-oic Acid Methyl Ester

Chemical Property:

Melting Point:99-100 °C
Boiling Point:505.7±25.0 °C(Predicted)
PKA:14.68±0.70(Predicted)
Density:1.085±0.06 g/cm3(Predicted)
Solubility.:Dichloromethane, Ethyl Acetate, Hexane

Purity/Quality:: (5β,6α)-6-Hydroxy-3-oxo-cholan-24-oicAcidMethylEster ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses 6α-Hydroxy bile acid analog. Used in the preparation of progesterone (P755900) and α-Hyodeoxycholic Acid (H998100). 6α-Hydroxy bile acid analog. (5β,6α)-6-Hydroxy-3-oxo-cholan-24-oic Acid Methyl Ester is used in the preparation of progesterone (P755900) and α-Hyodeoxycholic Acid (H998100).

Technology Process of (5β,6α)-6-Hydroxy-3-oxo-cholan-24-oic Acid Methyl Ester

There total 12 articles about (5β,6α)-6-Hydroxy-3-oxo-cholan-24-oic Acid Methyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 2868-48-6
methyl hyodeoxycholate

: 2862-62-6
3α-ol-6-oxo-5β-24-cholanoic acid methyl ester

: 3360-89-2
3α-oxo-6α-hydroxy-5β-cholan-24-oic acid methyl ester

Guidance literature:: With N-Bromosuccinimide; acetic acid; In water; acetone; at 0 - 20 ℃; for 1.16667h; Reagent/catalyst;
DOI:10.1055/s-0035-1560388

Reference yield: 83.0%

: 2868-48-6
methyl hyodeoxycholate

: 3360-89-2
3α-oxo-6α-hydroxy-5β-cholan-24-oic acid methyl ester

Guidance literature:: With N-Bromosuccinimide; acetic acid; In water; acetone; at 0 - 20 ℃; for 1.5h; regioselective reaction;
DOI:10.1016/j.steroids.2020.108594