2-bromo-4-[(methylsulfanyl){[(trimethysilyl)methyl]imino}methyl]benzyl acetate

Base Information

• Chemical Name: 2-bromo-4-[(methylsulfanyl){[(trimethysilyl)methyl]imino}methyl]benzyl acetate
• CAS No.: 1176331-10-4
• Molecular Formula: C₁₅H₂₂BrNO₂SSi
• Molecular Weight: 388.401

Synonyms:2-bromo-4-[(methylsulfanyl){[(trimethysilyl)methyl]imino}methyl]benzyl acetate

Chemical Property of 2-bromo-4-[(methylsulfanyl){[(trimethysilyl)methyl]imino}methyl]benzyl acetate

Chemical Property:

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Technology Process of 2-bromo-4-[(methylsulfanyl){[(trimethysilyl)methyl]imino}methyl]benzyl acetate

There total 1 articles about 2-bromo-4-[(methylsulfanyl){[(trimethysilyl)methyl]imino}methyl]benzyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-bromo-4-(2-oxopropyl)-N-trimethylsilanylmethylthiobenzamide (1174731-67-9) + methyl iodide (74-88-4) → 2-bromo-4-[(methylsulfanyl){[(trimethysilyl)methyl]imino}methyl]benzyl acetate (1176331-10-4)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield:

1,3-dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene (864725-22-4) + 2-bromo-4-[(methylsulfanyl){[(trimethysilyl)methyl]imino}methyl]benzyl acetate (1176331-10-4) → acetic acid 2-bromo-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]benzyl ester (1174731-68-0)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -5 - 20 ℃; Inert atmosphere;

upstream raw materials:

3-bromo-4-(2-oxopropyl)-N-trimethylsilanylmethylthiobenzamide

methyl iodide

Downstream raw materials:

acetic acid 2-bromo-4-[4-(3,5-dichlorophenyl)-4-trifluoromethyl-4,5-dihydro-3H-pyrrol-2-yl]benzyl ester

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