N-[3-[[2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)ethylmethylamino]methyl]phenyl]benzenesulphonamide

Base Information

Chemical Name:N-[3-[[2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)ethylmethylamino]methyl]phenyl]benzenesulphonamide
CAS No.:1459259-62-1
Molecular Formula:C₂₄H₂₆N₂O₅S
Molecular Weight:454.547
Hs Code.:

Synonyms:N-[3-[[2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)ethylmethylamino]methyl]phenyl]benzenesulphonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[3-[[2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)ethylmethylamino]methyl]phenyl]benzenesulphonamide

Chemical Property:

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Technology Process of N-[3-[[2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)ethylmethylamino]methyl]phenyl]benzenesulphonamide

There total 4 articles about N-[3-[[2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)ethylmethylamino]methyl]phenyl]benzenesulphonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1459261-63-2
3-({[2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)ethyl](methyl)amino}methyl)aniline

: 98-09-9
benzenesulfonyl chloride

: 1459259-62-1
N-[3-[[2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)ethylmethylamino]methyl]phenyl]benzenesulphonamide

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃;

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 1459259-62-1
N-[3-[[2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)ethylmethylamino]methyl]phenyl]benzenesulphonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanol; water / 1 h / 0 °C

1.2: 2 h / 0 - 20 °C

3.1: tin(ll) chloride; ethanol / 4 h / 60 °C

4.1: pyridine / dichloromethane / 20 °C

With pyridine; ethanol; tin(ll) chloride; In methanol; dichloromethane; water;

Reference yield:

: 19499-61-7
methyl-(3-nitro-benzyl)-amine

: 1459259-62-1
N-[3-[[2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)ethylmethylamino]methyl]phenyl]benzenesulphonamide

Guidance literature:: Multi-step reaction with 3 steps

2: tin(ll) chloride; ethanol / 4 h / 60 °C

3: pyridine / dichloromethane / 20 °C

With pyridine; ethanol; tin(ll) chloride; In dichloromethane;