2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)-N-metyl-N-(3-nitrobenzyl)ethylamine

Base Information

• Chemical Name: 2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)-N-metyl-N-(3-nitrobenzyl)ethylamine
• CAS No.: 1459261-59-6
• Molecular Formula: C₁₈H₂₀N₂O₅
• Molecular Weight: 344.367

Synonyms:2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)-N-metyl-N-(3-nitrobenzyl)ethylamine

Chemical Property of 2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)-N-metyl-N-(3-nitrobenzyl)ethylamine

Chemical Property:

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Technology Process of 2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)-N-metyl-N-(3-nitrobenzyl)ethylamine

There total 2 articles about 2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)-N-metyl-N-(3-nitrobenzyl)ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-nitro-benzaldehyde (99-61-6) → 2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)-N-metyl-N-(3-nitrobenzyl)ethylamine (1459261-59-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: methanol; water / 1 h / 0 °C

1.2: 2 h / 0 - 20 °C

In methanol; water;

Reference yield:

methyl-(3-nitro-benzyl)-amine (19499-61-7) + 5-(2-bromoethoxy)-2,3-dihydrobenzo[b][1,4]dioxine (1710-62-9) → 2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)-N-metyl-N-(3-nitrobenzyl)ethylamine (1459261-59-6)

Guidance literature:

Reference yield:

2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)-N-metyl-N-(3-nitrobenzyl)ethylamine (1459261-59-6) → 3-({[2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)ethyl](methyl)amino}methyl)aniline (1459261-63-2)

Guidance literature:

With ethanol; tin(ll) chloride; at 60 ℃; for 4h;

upstream raw materials:

3-nitro-benzaldehyde

methyl-(3-nitro-benzyl)-amine

5-(2-bromoethoxy)-2,3-dihydrobenzo[b][1,4]dioxine

Downstream raw materials:

N-[3-[[2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)ethylmethylamino]methyl]phenyl]benzenesulphonamide

3-({[2-(2,3-dihydro-1,4-benzodioxin-5-yloxy)ethyl](methyl)amino}methyl)aniline

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