methyl 3,4-di-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-xylopyranoside

Base Information

Chemical Name:methyl 3,4-di-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-xylopyranoside
CAS No.:1032715-88-0
Molecular Formula:C₂₅H₃₀O₈
Molecular Weight:458.508
Hs Code.:

Synonyms:methyl 3,4-di-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-xylopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3,4-di-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-xylopyranoside

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Technology Process of methyl 3,4-di-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-xylopyranoside

There total 1 articles about methyl 3,4-di-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 67-56-1
methanol

: 115220-82-1
(3R,4R)-3,4-Bis-benzyloxy-3,4-dihydro-2H-pyran

: 108-59-8
malonic acid dimethyl ester

: 1032715-88-0
methyl 3,4-di-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-xylopyranoside

: 1032715-89-1
methyl 3,4-di-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-α-D-lyxopyranoside

Guidance literature:: With ammonium cerium(IV) nitrate; sodium hydrogencarbonate; at 0 ℃;
DOI:10.1002/chem.200701151

Reference yield: 83.0%

: 1032715-88-0
methyl 3,4-di-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-xylopyranoside

: 1032716-00-9
methyl 3,4-di-O-benzyl-2-deoxy-2-C-[(methoxycarbonyl)methyl]-β-D-xylopyranoside

Guidance literature:: With lithium iodide; In dimethyl sulfoxide; at 100 ℃; under 7500.75 Torr; microwave irradiation;
DOI:10.1002/chem.200701151

Reference yield: 67.0%

: 1032715-88-0
methyl 3,4-di-O-benzyl-2-deoxy-2-C-[(bis-methoxycarbonyl)methyl]-β-D-xylopyranoside

: 1334529-22-4
C₂₃H₂₄O₇

Guidance literature:: With gold(III) tribromide; In water; acetonitrile; at 20 - 70 ℃; for 12h; stereoselective reaction; Inert atmosphere;
DOI:10.1039/c1cc13425f