1-(1-Ethoxy-ethoxy)-3-methoxymethoxy-2-methylene-cyclohexanecarbonitrile

Base Information

Chemical Name:1-(1-Ethoxy-ethoxy)-3-methoxymethoxy-2-methylene-cyclohexanecarbonitrile
CAS No.:77406-99-6
Molecular Formula:C₁₄H₂₃NO₄
Molecular Weight:269.341
Hs Code.:

Synonyms:1-(1-Ethoxy-ethoxy)-3-methoxymethoxy-2-methylene-cyclohexanecarbonitrile

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Chemical Property of 1-(1-Ethoxy-ethoxy)-3-methoxymethoxy-2-methylene-cyclohexanecarbonitrile

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Technology Process of 1-(1-Ethoxy-ethoxy)-3-methoxymethoxy-2-methylene-cyclohexanecarbonitrile

There total 5 articles about 1-(1-Ethoxy-ethoxy)-3-methoxymethoxy-2-methylene-cyclohexanecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 77406-98-5
2-(1-Ethoxy-ethoxy)-7-iodo-4-methoxymethoxy-3-methylene-heptanenitrile

: 77406-99-6
1-(1-Ethoxy-ethoxy)-3-methoxymethoxy-2-methylene-cyclohexanecarbonitrile

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at 40 ℃; for 1.5h;
DOI:10.1016/0040-4039(81)80164-5

Reference yield:

: 77406-95-2
6-Iodo-3-methoxymethoxy-2-methylene-hexanal

: 77406-99-6
1-(1-Ethoxy-ethoxy)-3-methoxymethoxy-2-methylene-cyclohexanecarbonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: ZnI₂ / 1 h / warmed from 0 deg C to room temperature

2: 3N HCl / tetrahydrofuran / 0.25 h / 0 °C

3: p-TsOH / benzene

4: 79 percent / sodium hexamethyldisilazane / tetrahydrofuran / 1.5 h / 40 °C

With hydrogenchloride; sodium hexamethyldisilazane; toluene-4-sulfonic acid; zinc(II) iodide; In tetrahydrofuran; benzene;
DOI:10.1016/0040-4039(81)80164-5

Reference yield:

: 77406-94-1
2-Diethoxymethyl-6-iodo-hex-1-en-3-ol

: 77406-99-6
1-(1-Ethoxy-ethoxy)-3-methoxymethoxy-2-methylene-cyclohexanecarbonitrile

Guidance literature:: Multi-step reaction with 5 steps

1: 2.) copper sulfate / 1.) diethylaniline, room temperature, 12 h, 2.) methanol-water, room temperature, 1 h

2: ZnI₂ / 1 h / warmed from 0 deg C to room temperature

3: 3N HCl / tetrahydrofuran / 0.25 h / 0 °C

4: p-TsOH / benzene

5: 79 percent / sodium hexamethyldisilazane / tetrahydrofuran / 1.5 h / 40 °C

With hydrogenchloride; copper(I) sulfate; sodium hexamethyldisilazane; toluene-4-sulfonic acid; zinc(II) iodide; In tetrahydrofuran; benzene;
DOI:10.1016/0040-4039(81)80164-5