2-Aza-bicyclo[2.1.1]hexane-1-carboxylic acid benzyl ester; compound with toluene-4-sulfonic acid

Base Information

Chemical Name:2-Aza-bicyclo[2.1.1]hexane-1-carboxylic acid benzyl ester; compound with toluene-4-sulfonic acid
CAS No.:103794-05-4
Molecular Formula:C₇H₈O₃S*C₁₃H₁₅NO₂
Molecular Weight:389.472
Hs Code.:

Synonyms:2-Aza-bicyclo[2.1.1]hexane-1-carboxylic acid benzyl ester; compound with toluene-4-sulfonic acid

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Chemical Property of 2-Aza-bicyclo[2.1.1]hexane-1-carboxylic acid benzyl ester; compound with toluene-4-sulfonic acid

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Technology Process of 2-Aza-bicyclo[2.1.1]hexane-1-carboxylic acid benzyl ester; compound with toluene-4-sulfonic acid

There total 1 articles about 2-Aza-bicyclo[2.1.1]hexane-1-carboxylic acid benzyl ester; compound with toluene-4-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73550-56-8
2-azabicyclo[2.1.1]hexane-1-carboxylic acid

: 104-15-4
toluene-4-sulfonic acid

: 100-51-6,185532-71-2
benzyl alcohol

: 103794-05-4
2-Aza-bicyclo[2.1.1]hexane-1-carboxylic acid benzyl ester; compound with toluene-4-sulfonic acid

Guidance literature:: In benzene; for 16h; Heating;
DOI:10.1021/ja00281a051

Reference yield: 96.0%

: 103794-05-4
2-Aza-bicyclo[2.1.1]hexane-1-carboxylic acid benzyl ester; compound with toluene-4-sulfonic acid

: 74-89-5
methylamine

: 103794-07-6
2,4-MePro-NHMe

Guidance literature:: In water; for 3h; Heating;
DOI:10.1021/ja00281a051

Reference yield:

: 103794-05-4
2-Aza-bicyclo[2.1.1]hexane-1-carboxylic acid benzyl ester; compound with toluene-4-sulfonic acid

: 103794-09-8
L-Tyr-2,4-MePro-NHMe

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / H₂O / 3 h / Heating

2: 70 percent / DCC / dimethylformamide / 3 h / Ambient temperature

3: 30percent trifluoroacetic acid / CH₂Cl₂ / 3 h / Ambient temperature

With dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja00281a051