(Z)-α-phenoxybutenoic acid

Base Information

Chemical Name:(Z)-α-phenoxybutenoic acid
CAS No.:937025-54-2
Molecular Formula:C₁₀H₁₀O₃
Molecular Weight:178.188
Hs Code.:

Synonyms:(Z)-α-phenoxybutenoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-α-phenoxybutenoic acid

Chemical Property:

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Technology Process of (Z)-α-phenoxybutenoic acid

There total 3 articles about (Z)-α-phenoxybutenoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 1746-13-0
allyl phenyl ether

: 937025-54-2
(Z)-α-phenoxybutenoic acid

Guidance literature:: allyl phenyl ether; With 2,2,6,6-tetramethylpiperidinyl-lithium; triisobutylaluminum; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 3h; Inert atmosphere;

carbon dioxide; With [(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)Cu(O-tBu)]; In tetrahydrofuran; at -78 - 0 ℃; for 2h; under 760.051 Torr; regioselective reaction; Further stages; Inert atmosphere;
DOI:10.1039/c7ob00341b

Reference yield:

: methyl 2-phenyloxy-(Z)-2-butenoate

: 937025-54-2
(Z)-α-phenoxybutenoic acid

Guidance literature:: With potassium hydroxide; In water; at 22 ℃; for 20h;
DOI:10.1021/ol0488035

Reference yield:

: 108-95-2,27073-41-2
phenol

: 937025-54-2
(Z)-α-phenoxybutenoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / acetonitrile / 16 h / 80 °C

2: KOH / H₂O / 20 h / 22 °C

With potassium hydroxide; potassium carbonate; In water; acetonitrile;
DOI:10.1021/ol0488035