3-(2-Hydroxy-1-naphthylmethyleneamino)benzoic acid

Base Information

Chemical Name:3-(2-Hydroxy-1-naphthylmethyleneamino)benzoic acid
CAS No.:88826-07-7
Molecular Formula:C₁₈H₁₃NO₃
Molecular Weight:291.306
Hs Code.:
European Community (EC) Number:667-241-7
Nikkaji Number:J1.440.274H,J3.095.337A
ChEMBL ID:CHEMBL4225473

Synonyms:88826-07-7;3-(((2-Hydroxynaphthalen-1-yl)methylene)amino)benzoic acid;SCHEMBL7824843;CHEMBL4225473;SCHEMBL22750721;3-(2-HYDROXY-1-NAPHTHYLMETHYLENEAMINO)BENZOIC ACID;AKOS024335226;N-(3-Carboxy-phenyl)-2-hydroxy-1-naphthaldimine;3-[(E)-[(2-hydroxynaphthalen-1-yl)methylidene]amino]benzoic acid

Suppliers and Price of 3-(2-Hydroxy-1-naphthylmethyleneamino)benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-(2-Hydroxy-1-naphthylmethyleneamino)benzoic acid

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:291.08954328
Heavy Atom Count:22
Complexity:423

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=CC(=C2C=NC3=CC=CC(=C3)C(=O)O)O

Technology Process of 3-(2-Hydroxy-1-naphthylmethyleneamino)benzoic acid

There total 1 articles about 3-(2-Hydroxy-1-naphthylmethyleneamino)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-05-8,159139-79-4
meta-aminobenzoic acid

: 708-06-5
2-hydroxynaphthalene-1-carbaldehyde

: 88826-07-7
3-(((2-hydroxynaphthalen-1-yl)methylene)amino)benzoic acid

Guidance literature:: With ethanol;

Reference yield: 83.0%

: 88826-07-7
3-(((2-hydroxynaphthalen-1-yl)methylene)amino)benzoic acid

: 1066-45-1
trimethyltin(IV)chloride

: (C₁₀H₆(OH)CHNC₆H₄(COO))Sn(CH₃)3

Guidance literature:: With EtONa; In methanol; N2; ligand and EtONa refluxed in MeOH for 30 min, Sn compd. added (1:1:1molar ratio), mixt. refluxed for 8 h; filtered, evapd., recrystd. (DCM/petroleum ether=1.5/1, v/v), elem. anal.;
DOI:10.1016/j.jorganchem.2012.03.027

Reference yield: 80.0%

: 64-17-5
ethanol

: 88826-07-7
3-(((2-hydroxynaphthalen-1-yl)methylene)amino)benzoic acid

: 683-18-1
dibutyltin chloride

: 2C₁₀H₆(OH)CHNC₆H₄(CO₂)^(1-)*2C₄H₉^(1-)*Sn⁽⁴⁺⁾*C₂H₅OH=[(C₁₀H₆(OH)CHNC₆H₄(COO))2(Sn(C₄H₉)2)]*C₂H₅OH

Guidance literature:: With EtONa; In methanol; N2; ligand and EtONa refluxed in MeOH for 30 min, Sn compd. added (2:2:1molar ratio), mixt. refluxed for 8 h; filtered, evapd., recrystd. (DCM/petroleum ether=1/1, v/v), elem. anal.;
DOI:10.1016/j.jorganchem.2012.03.027