N-methyl rolipram

Base Information

Chemical Name:N-methyl rolipram
CAS No.:1443535-38-3
Molecular Formula:C₁₇H₂₃NO₃
Molecular Weight:289.375
Hs Code.:

Synonyms:N-methyl rolipram

Suppliers and Price of N-methyl rolipram

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of N-methyl rolipram

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of N-methyl rolipram

There total 3 articles about N-methyl rolipram which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 67-56-1
methanol

: 1021867-92-4,138715-52-3
methyl 3-(3-cyclopentyloxy-4-methoxyphenyl)-4-nitrobutanoate

: 61413-54-5
Rolipram

: 1443535-38-3
N-methyl rolipram

Guidance literature:: With palladium 10% on activated carbon; hydrogen; at 60 ℃; for 5h; under 7500.75 Torr; Autoclave; Inert atmosphere;
DOI:10.1055/s-0032-1316874

Reference yield:

: 1021867-92-4,138715-52-3
methyl 3-(3-cyclopentyloxy-4-methoxyphenyl)-4-nitrobutanoate

: 61413-54-5
Rolipram

: 1443535-38-3
N-methyl rolipram

: 1443535-39-4
C₁₉H₂₉NO₄

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; water; at 20 ℃; under 37503.8 Torr; Autoclave; Inert atmosphere;
DOI:10.1055/s-0032-1316874

Reference yield:

: 61413-54-5
Rolipram

: 74-88-4
methyl iodide

: 1443535-38-3
N-methyl rolipram

Guidance literature:: Rolipram; In tetrahydrofuran; at 0 ℃; for 0.5h;

With lithium diisopropyl amide; In tetrahydrofuran; at 0 ℃;

methyl iodide; In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.2174/1386207322666190306142810