trimethyl[(1S)-1-methyl-3-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propyl]silane

Base Information

Chemical Name:trimethyl[(1S)-1-methyl-3-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propyl]silane
CAS No.:1270304-83-0
Molecular Formula:C₁₉H₃₃BO₂Si
Molecular Weight:332.366
Hs Code.:

Synonyms:trimethyl[(1S)-1-methyl-3-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propyl]silane

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Chemical Property of trimethyl[(1S)-1-methyl-3-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propyl]silane

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Technology Process of trimethyl[(1S)-1-methyl-3-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propyl]silane

There total 1 articles about trimethyl[(1S)-1-methyl-3-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propyl]silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1270304-91-0
3-phenyl-1-(trimethylsilyl)propyl diisopropylcarbamate

: 94242-85-0
2,4,4,5,5-pentamethyl-[1,3,2]dioxaborolane

: 1270304-83-0
trimethyl[(1S)-1-methyl-3-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propyl]silane

Guidance literature:: 3-phenyl-1-(trimethylsilyl)propyl diisopropylcarbamate; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In diethyl ether; cyclohexane; at -78 ℃; for 5h; Inert atmosphere;

2,4,4,5,5-pentamethyl-[1,3,2]dioxaborolane; In diethyl ether; cyclohexane; at -78 ℃; Inert atmosphere; Reflux;
DOI:10.1021/ol200177f

Reference yield: 73.0%

: 1270304-83-0
trimethyl[(1S)-1-methyl-3-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propyl]silane

: 917-57-7
vinyllithium

: 1270304-88-5
[(1S)-1-ethyl-1-(2-phenylethyl)prop-2-en-1-yl](trimethyl)silane

Guidance literature:: trimethyl[(1S)-1-methyl-3-phenyl-1-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)propyl]silane; vinyllithium; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

With iodine; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol200177f